[(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3]

Base Information

Chemical Name:[(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3]
CAS No.:1358811-13-8
Molecular Formula:C₁₃H₂₀BNO₂*C₁₈HBF₁₅*H
Molecular Weight:747.119
Hs Code.:

Synonyms:[(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3]

Suppliers and Price of [(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3]

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of [(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3]

Chemical Property:

Purity/Quality:: 98%min ^*data from raw suppliers

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Technology Process of [(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3]

There total 1 articles about [(2,6-Me2)(4-Bpin)C5H2NH][HB(C6F5)3] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1109-15-5
tris(pentafluorophenyl)borate

: 1333-74-0
hydrogen

: 325142-95-8
2,6-dimethyl-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine

: 1358811-13-8
[(2,6-Me₂)(4-Bpin)C₅H₂NH][HB(C₆F₅)3]

Guidance literature:: In toluene; High Pressure; soln. B(C6F5)3 in toluene was added to soln. pyridine in toluene, soln. was freeze-pump thawed for 3 cycles and backfilled with H2 77 K (4 atm),stirred overnight; soln. was pumped to dryness, residue was washed with pentane, crysn. from toluene; elem. anal.;
DOI:10.1039/c1dt11820j