4-(Boc-aMinoethyloxy)benzonitrile

Base Information

• Chemical Name: 4-(Boc-aMinoethyloxy)benzonitrile
• CAS No.: 919085-52-2
• Molecular Formula: C14H18N2O3
• Molecular Weight: 262.309
• Hs Code.: 2926907090
• Mol file: 919085-52-2.mol

Synonyms:4-(Boc-aMinoethyloxy)benzonitrile;2-Methyl-2-propanyl [2-(4-cyanophenoxy)ethyl]carbamate

Chemical Property of 4-(Boc-aMinoethyloxy)benzonitrile

Chemical Property:

• PSA: 74.84000
• LogP: 2.66618

Purity/Quality:

97% ^*data from raw suppliers

4-(Boc-aminoethyloxy)benzonitrile ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-(Boc-aMinoethyloxy)benzonitrile

There total 4 articles about 4-(Boc-aMinoethyloxy)benzonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

2-(N-tert-butoxycarbonylamino)ethanol (26690-80-2) + 4-cyanophenol (767-00-0) → tert-butyl (2-(4-cyanophenoxy)ethyl)carbamate (919085-52-2)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 5 - 100 ℃; for 8.16667h;

DOI:10.1016/j.bmcl.2014.12.008

Reference yield: 73.0%

2-(tert-butoxycarbonylamino)ethyl bromide (39684-80-5) + 4-cyanophenol (767-00-0) → tert-butyl (2-(4-cyanophenoxy)ethyl)carbamate (919085-52-2)

Guidance literature:

4-cyanophenol; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

2-(tert-butoxycarbonylamino)ethyl bromide; In N,N-dimethyl-formamide; at 20 ℃;

Reference yield: 20.09%

2-(tert-butoxycarbonylamino)ethyl methanesulfonate (96628-67-0) + 4-cyanophenol (767-00-0) → tert-butyl (2-(4-cyanophenoxy)ethyl)carbamate (919085-52-2)

Guidance literature:

4-cyanophenol; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

2-(tert-butoxycarbonylamino)ethyl methanesulfonate; In N,N-dimethyl-formamide; at 100 ℃; for 16h;

upstream raw materials:

2-(tert-butoxycarbonylamino)ethyl bromide

4-cyanophenol

2-(N-tert-butoxycarbonylamino)ethanol

2-(tert-butoxycarbonylamino)ethyl methanesulfonate

Downstream raw materials:

C₁₅H₂₀N₄O₃

4-(2-aminoethoxy)benzonitrile

C₂₃H₂₇N₅O₄

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