Ethyl 4-methoxy-3,5-dimethylbenzoylformate

Base Information

• Chemical Name: Ethyl 4-methoxy-3,5-dimethylbenzoylformate
• CAS No.: 107642-57-9
• Molecular Formula: C₁₃H₁₆O₄
• Molecular Weight: 236.268
• Hs Code.: 2918990090
• European Community (EC) Number: 675-594-3
• DSSTox Substance ID: DTXSID80374534
• Wikidata: Q82163152
• Mol file: 107642-57-9.mol

Synonyms:107642-57-9;Ethyl 4-methoxy-3,5-dimethylbenzoylformate;ethyl 2-(4-methoxy-3,5-dimethylphenyl)-2-oxoacetate;ethyl 3,5-dimethyl-4-methoxybenzoylformate;DTXSID80374534;MFCD06201703;AKOS016017109;FS-3939;CS-0364602;ethyl2-(4-methoxy-3,5-dimethylphenyl)-2-oxoacetate;ethyl 4-methoxy-3,5-dimethylbenzoylformate, AldrichCPR

Chemical Property of Ethyl 4-methoxy-3,5-dimethylbenzoylformate

Chemical Property:

• Vapor Pressure: 2.02E-05mmHg at 25°C
• Boiling Point: 361.8°C at 760 mmHg
• Flash Point: 159.6°C
• PSA: 52.60000
• Density: 1.103g/cm³
• LogP: 2.05780
• XLogP3: 2.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 236.10485899
• Heavy Atom Count: 17
• Complexity: 275

Purity/Quality:

95% ^*data from raw suppliers

(4-Methoxy-3,5-dimethylphenyl)oxoaceticacidethylester ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xn
• Statements: 22-36
• Safety Statements: 26

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)C(=O)C1=CC(=C(C(=C1)C)OC)C

Technology Process of Ethyl 4-methoxy-3,5-dimethylbenzoylformate

There total 1 articles about Ethyl 4-methoxy-3,5-dimethylbenzoylformate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-methoxy-1,3-dimethylbenzene (1004-66-6) + Ethyl oxalyl chloride (4755-77-5) → ethyl 4-methoxy-3,5-dimethylphenylglyoxylate (107642-57-9)

Guidance literature:

With aluminium trichloride; In chloroform; for 1h; Ambient temperature;

Reference yield: 64.0%

(2,6-dimethylphenyl)hydrazine (603-77-0) + ethyl 4-methoxy-3,5-dimethylphenylglyoxylate (107642-57-9) → [(2,6-Dimethyl-phenyl)-hydrazono]-(4-methoxy-3,5-dimethyl-phenyl)-acetic acid ethyl ester (107642-58-0)

Guidance literature:

With acetic acid; In ethanol; for 0.166667h; Heating;

Reference yield:

ethyl 4-methoxy-3,5-dimethylphenylglyoxylate (107642-57-9) → (4-methoxy-3,5-dimethylphenyl)(2-methylquinolin-4-yl)methanone

Guidance literature:

Multi-step reaction with 2 steps

1: sodium hydroxide; water / 6 h / 20 °C

2: dipotassium peroxodisulfate / acetonitrile; water / 15 h / 20 - 37 °C / Irradiation; Green chemistry

With dipotassium peroxodisulfate; water; sodium hydroxide; In water; acetonitrile;

DOI:10.1002/adsc.201800692

upstream raw materials:

2-methoxy-1,3-dimethylbenzene

Ethyl oxalyl chloride

Downstream raw materials:

[(2,6-Dimethyl-phenyl)-hydrazono]-(4-methoxy-3,5-dimethyl-phenyl)-acetic acid ethyl ester

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 107642-57-9 ETHYL 4-METHOXY-3,5-DIMETHYLBENZOYLFORMATE

Send

Send

Metric Ton KG G Pound L ML

Send

Send