3-diMethylbenzyl)cyclopropanaMine hydrochloride

Base Information

• Chemical Name: 3-diMethylbenzyl)cyclopropanaMine hydrochloride
• CAS No.: 909702-86-9
• Molecular Formula: C12H18ClN
• Molecular Weight: 211.735
• Hs Code.: 2921490090
• Mol file: 909702-86-9.mol

Synonyms:3-diMethylbenzyl)cyclopropanaMine hydrochloride;BenzeneMethanaMine, N-cyclopropyl-2,3-diMethyl-, hydrochloride;N-Cyclopropyl-2,3-dimethylbenzylamine hydrochloride, 3-[(Cyclopropylamino)methyl]-o-xylene hydrochloride

Chemical Property of 3-diMethylbenzyl)cyclopropanaMine hydrochloride

Chemical Property:

• PSA: 12.03000
• LogP: 3.74830
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

N-Cyclopropyl2,3-dimethylbenzylamineHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-diMethylbenzyl)cyclopropanaMine hydrochloride

There total 1 articles about 3-diMethylbenzyl)cyclopropanaMine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclopropyl-(2,3-dimethyl-benzyl)-amine (625437-38-9) → N-(2,3-dimethylbenzyl)cyclopropanamine hydrochloride (909702-86-9)

Guidance literature:

With hydrogenchloride; In diethyl ether; tert-butyl methyl ether; at 5 ℃; Product distribution / selectivity;

Reference yield: 100.0%

N-(2,3-dimethylbenzyl)cyclopropanamine hydrochloride (909702-86-9) + (rac.)-(3aR*,6aR*)-5-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-3,3a,6,6a-tetrahydro-1H-cyclopenta[c]pyrrole-2,4-dicarboxylic acid 2-tert-butyl ester → (rac.)-(3aR*,6aR*)-5-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-6-[cyclopropyl-(2,3-dimethyl-benzyl)-carbamoyl]-3,3a,4,6a-tetrahydro-1H-cyclopenta[c]pyrrole-2-carboxylic acid tert-butyl ester

Guidance literature:

(rac.)-(3aR*,6aR*)-5-{4-[3-(tert-butyl-dimethyl-silanyloxy)-propyl]-phenyl}-3,3a,6,6a-tetrahydro-1H-cyclopenta[c]pyrrole-2,4-dicarboxylic acid 2-tert-butyl ester; With 4-methyl-morpholine; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; at 20 ℃; for 0.25h;

N-(2,3-dimethylbenzyl)cyclopropanamine hydrochloride; In N,N-dimethyl-formamide; for 16h;

Reference yield: 95.0%

N-(2,3-dimethylbenzyl)cyclopropanamine hydrochloride (909702-86-9) + acetyl chloride (75-36-5) → cyclopropyl-2,3-dimethylbenzylacetamide (1041438-90-7)

Guidance literature:

With potassium carbonate; In tert-butyl methyl ether; water; at 5 - 25 ℃;

upstream raw materials:

cyclopropyl-(2,3-dimethyl-benzyl)-amine

Downstream raw materials:

cyclopropyl-2,3-dimethylbenzylacetamide

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