1(10)-Aristolen-2-one

Base Information

• Chemical Name: 1(10)-Aristolen-2-one
• CAS No.: 28398-06-3
• Molecular Formula: C15H22O
• Molecular Weight: 218.33
• Mol file: 28398-06-3.mol

Synonyms:1(10)-Aristolen-2-one;(1aR)-1,1,7β,7aβ-Tetramethyl-1aβ,2,3,5,6,7,7a,7bβ-octahydro-1H-cyclopropa[a]naphthalene-5-one;[1aR,(+)]-1,1aβ,2,3,6,7,7a,7bβ-Octahydro-1,1,7β,7aβ-tetramethyl-5H-cyclopropa[a]naphthalen-5-one

Chemical Property of 1(10)-Aristolen-2-one

Chemical Property:

• Melting Point: 41 °C
• PSA: 17.07000
• LogP: 3.59400

Purity/Quality:

99% ^*data from raw suppliers

1(10)-Aristolen-2-one ≥98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
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Technology Process of 1(10)-Aristolen-2-one

There total 4 articles about 1(10)-Aristolen-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

(1aR)-5ξ-hydroxy-1.1.7c.7ac-tetramethyl-(1arH.7bcH)-1a.2.3.5.6.7.7a.7b-octahydro-1H-cyclopropa[a]naphthalene (77381-79-4,145988-07-4) → (1aR)-5-oxo-1.1.7c.7ac-tetramethyl-(1arH.7bcH)-1a.2.3.5.6.7.7a.7b-octahydro-1H-cyclopropa[a]naphthalene (28398-06-3,808102-61-6)

Guidance literature:

With chromium(VI) oxide; sulfuric acid; In acetone; for 0.0833333h;

DOI:10.1246/bcsj.53.3721

Reference yield: 18.7%

β-gurjunene (17334-55-3) → aristolone (3293-43-4,6831-17-0,20536-71-4,22419-46-1,25274-27-5,27779-52-8) + (1aR)-5-oxo-1.1.7c.7ac-tetramethyl-(1arH.7bcH)-1a.2.3.5.6.7.7a.7b-octahydro-1H-cyclopropa[a]naphthalene (28398-06-3,808102-61-6) + (1aR,3R,7R,7aR,7bS)-3-hydroxy-1,1,7,7a-tetramethyl-1,1a,2,3,6,7,7a,7b-octahydro-5H-cyclopropa[α]naphthalen-5-one (26808-51-5)

Guidance literature:

With culture medium of Chlorella fusca var. vacuocola IAMC-28; Noro medium; at 25 ℃; for 528h;

DOI:10.1248/cpb.54.861

Reference yield:

β-gurjunene (17334-55-3) → (1aR)-5-oxo-1.1.7c.7ac-tetramethyl-(1arH.7bcH)-1a.2.3.5.6.7.7a.7b-octahydro-1H-cyclopropa[a]naphthalene (28398-06-3,808102-61-6)

Guidance literature:

With sodium chromate(VI); In acetic acid;

upstream raw materials:

β-gurjunene

(1aR)-5ξ-hydroxy-1.1.7c.7ac-tetramethyl-(1arH.7bcH)-1a.2.3.5.6.7.7a.7b-octahydro-1H-cyclopropa[a]naphthalene

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