4-(Trimethylsiloxy)phenylacetic acid methyl ester

Base Information

Chemical Name:4-(Trimethylsiloxy)phenylacetic acid methyl ester
CAS No.:27798-62-5
Molecular Formula:C₁₂H₁₈O₃Si
Molecular Weight:238.359
Hs Code.:2931900090
Mol file:27798-62-5.mol

Synonyms:4-(Trimethylsiloxy)phenylacetic acid methyl ester;p-(Trimethylsiloxy)benzeneacetic acid methyl ester

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(Trimethylsiloxy)phenylacetic acid methyl ester

Chemical Property:

PSA：35.53000
LogP:2.61580

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-(Trimethylsiloxy)phenylacetic acid methyl ester

There total 1 articles about 4-(Trimethylsiloxy)phenylacetic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 14199-15-6
Methyl 4-hydroxyphenylacetate

: 27798-62-5
methyl 4-(trimethylsilyloxy)phenylacetate

Guidance literature:: With triethylamine; In tetrahydrofuran; at 20 ℃; for 15h;
DOI:10.1021/jo048403v

Reference yield: 81.0%

: 27798-62-5
methyl 4-(trimethylsilyloxy)phenylacetate

: 75-05-8,26809-02-9
acetonitrile

: methyl 2-(1-acetamido-4-oxocyclohexa-2,5-dien-1-yl)acetate

Guidance literature:: With [bis(acetoxy)iodo]benzene; trifluoroacetic acid;
DOI:10.1021/jo800267q

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 27798-62-5
methyl 4-(trimethylsilyloxy)phenylacetate

: 1-methoxy-1-(trimethylsilyloxy)-2-(4-trimethylsilyloxyphenyl)ethylene

: 1-methoxy-1-(trimethylsilyloxy)-2-(4-trimethylsilyloxyphenyl)ethylene

Guidance literature:: methyl 4-(trimethylsilyloxy)phenylacetate; With lithium diisopropyl amide; In tetrahydrofuran; hexane; at -78 ℃; for 1h;

chloro-trimethyl-silane; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 15h; Title compound not separated from byproducts;
DOI:10.1021/jo048403v