(R)-tert-butyl 1-(4-iodophenylamino)-1-oxopropan-2-ylcarbamate

Base Information

Chemical Name:(R)-tert-butyl 1-(4-iodophenylamino)-1-oxopropan-2-ylcarbamate
CAS No.:1352083-14-7
Molecular Formula:C₁₄H₁₉IN₂O₃
Molecular Weight:390.221
Hs Code.:
Mol file:1352083-14-7.mol

Synonyms:(R)-tert-butyl 1-(4-iodophenylamino)-1-oxopropan-2-ylcarbamate

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Chemical Property of (R)-tert-butyl 1-(4-iodophenylamino)-1-oxopropan-2-ylcarbamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of (R)-tert-butyl 1-(4-iodophenylamino)-1-oxopropan-2-ylcarbamate

There total 1 articles about (R)-tert-butyl 1-(4-iodophenylamino)-1-oxopropan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 3744-87-4,7764-95-6,15761-38-3
Boc-(R)-Ala

: 540-37-4
p-aminoiodobenzene

: 1352083-14-7
tert-butyl {(2R)-1-[(4-iodophenyl)amino]-1-oxopropan-2-yl}carbamate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; HATU; In N,N-dimethyl-formamide; at 20 ℃; for 1h; Inert atmosphere;

Reference yield: 52.0%

: 1352083-14-7
tert-butyl {(2R)-1-[(4-iodophenyl)amino]-1-oxopropan-2-yl}carbamate

: 1692-15-5
4-pyridylboronic acid

: 1352083-15-8
tert-butyl [(2R)-1-oxo-1-{[4-(pyridin-4-yl)phenyl]amino}propan-2-yl]carbamate

Guidance literature:: With sodium carbonate; palladium diacetate; triphenylphosphine; In 1,4-dioxane; water; at 100 ℃; for 2h; Inert atmosphere;

Reference yield:

: 1352083-14-7
tert-butyl {(2R)-1-[(4-iodophenyl)amino]-1-oxopropan-2-yl}carbamate

: 1352083-16-9
N-[4-(pyridin-4-yl)phenyl]-D-alaninamide hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate / triphenylphosphine; palladium diacetate / 1,4-dioxane; water / 2 h / 100 °C / Inert atmosphere

2: hydrogenchloride / 1,4-dioxane / 1.5 h / 20 °C

With hydrogenchloride; sodium carbonate; palladium diacetate; triphenylphosphine; In 1,4-dioxane; water;