Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)-

Base Information

Chemical Name:Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)-
CAS No.:1334763-80-2
Molecular Formula:C₁₆H₁₃N₃O
Molecular Weight:263.299
Hs Code.:2933990090
Mol file:1334763-80-2.mol

Synonyms:Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)-;1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)ethanone

Suppliers and Price of Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-(6-Methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethanone 95+%
1g
$ 772.00

Chemenu
1-(6-methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethan-1-one 95%
1g
$ 729.00

American Custom Chemicals Corporation
1-(6-METHYLPYRIDIN-2-YL)-2-(QUINOXALIN-6-YL)ETHANONE 95.00%
5MG
$ 497.72

Alichem
1-(6-Methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethanone
1g
$ 640.56

Total 7 raw suppliers

Chemical Property of Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)-

Chemical Property:

Melting Point:128.6 °C
Boiling Point:448.8±40.0 °C(Predicted)
PKA:2.78±0.10(Predicted)
PSA：55.74000
Density:1.243±0.06 g/cm3(Predicted)
LogP:2.75860
Storage Temp.:2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

1-(6-Methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethanone 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)-

There total 1 articles about Ethanone, 1-(6-Methyl-2-pyridinyl)-2-(6-quinoxalinyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 614750-85-5
diphenyl (6-methylpyridin-2-yl)(phenylamino)methylphosphonate

: 130345-50-5
quinoxaline-6-carbaldehyde

: 1334763-80-2
1-(6-methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethanone

Guidance literature:: diphenyl (6-methylpyridin-2-yl)(phenylamino)methylphosphonate; quinoxaline-6-carbaldehyde; With caesium carbonate; In tetrahydrofuran; isopropyl alcohol; at 20 ℃; for 16h;

With hydrogenchloride; In tetrahydrofuran; water; isopropyl alcohol; for 1h;

With potassium hydroxide; In water; pH=7 - 8;
DOI:10.1016/j.ejmech.2011.05.063

Reference yield:

: 1334763-80-2
1-(6-methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethanone

: 1334764-13-4
3-{2-[3-(6-methylpyridin-2-yl)-4-(quinoxalin-6-yl)-1H-pyrazol-1-yl]acetamido}benzamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: acetic acid / N,N-dimethyl-formamide / 2 h / 80 °C

1.2: 4 h / Reflux

2.1: sodium hydride; sodium iodide / N,N-dimethyl-formamide / 2 h / 20 °C

3.1: Lawessons reagent / 1,2-dimethoxyethane / 12 h / 85 °C

4.1: dihydrogen peroxide; sodium hydroxide / ethanol / 4 h / 40 °C

With Lawessons reagent; dihydrogen peroxide; sodium hydride; acetic acid; sodium iodide; sodium hydroxide; In 1,2-dimethoxyethane; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.05.063

Reference yield:

: 1334763-80-2
1-(6-methylpyridin-2-yl)-2-(quinoxalin-6-yl)ethanone

: 1334763-93-7
N-(3-cyanophenyl)-2-[3-(6-methylpyridin-2-yl)-4-(quinoxalin-6-yl)-1H-pyrazol-1-yl]acetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / N,N-dimethyl-formamide / 2 h / 80 °C

1.2: 4 h / Reflux

2.1: sodium hydride; sodium iodide / N,N-dimethyl-formamide / 2 h / 20 °C

With sodium hydride; acetic acid; sodium iodide; In N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2011.05.063