3-(1,3-Dioxolan-2-YL)benzophenone

Base Information

Chemical Name:3-(1,3-Dioxolan-2-YL)benzophenone
CAS No.:85366-46-7
Molecular Formula:C16H14O3
Molecular Weight:254.285
Hs Code.:2932999099
DSSTox Substance ID:DTXSID50441141
Wikidata:Q82257761
Mol file:85366-46-7.mol

Synonyms:3-(1,3-DIOXOLAN-2-YL)BENZOPHENONE;85366-46-7;[3-(1,3-dioxolan-2-yl)phenyl]-phenylmethanone;MFCD02260438;SCHEMBL2539492;DTXSID50441141;NZPRGYBCSLSUOM-UHFFFAOYSA-N;2-(3-benzoylphenyl)-1,3-dioxolane;AKOS016022086;(3-[1,3]Dioxolan-2-ylphenyl)phenylmethanone;A914822

Suppliers and Price of 3-(1,3-Dioxolan-2-YL)benzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
3-(1,3-Dioxolan-2-yl)benzophenone 97%
1g
$ 417.00

Rieke Metals
3-(1,3-Dioxolan-2-yl)benzophenone 97%
5g
$ 1514.00

Rieke Metals
3-(1,3-Dioxolan-2-yl)benzophenone 97%
2g
$ 731.00

Matrix Scientific
3-(1,3-Dioxolan-2-yl)benzophenone
1g
$ 437.00

Crysdot
3-(1,3-Dioxolan-2-yl)benzophenone 95+%
1g
$ 433.00

Crysdot
3-(1,3-Dioxolan-2-yl)benzophenone 95+%
5g
$ 1401.00

American Custom Chemicals Corporation
3-(1,3-DIOXOLAN-2-YL)BENZOPHENONE 95.00%
10G
$ 3395.70

American Custom Chemicals Corporation
3-(1,3-DIOXOLAN-2-YL)BENZOPHENONE 95.00%
5G
$ 2243.59

American Custom Chemicals Corporation
3-(1,3-DIOXOLAN-2-YL)BENZOPHENONE 95.00%
1G
$ 1006.58

Total 5 raw suppliers

Chemical Property of 3-(1,3-Dioxolan-2-YL)benzophenone

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:409.674°C at 760 mmHg
Flash Point:193.235°C
PSA：35.53000
Density:1.193g/cm³
LogP:2.96300
XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:254.094294304
Heavy Atom Count:19
Complexity:303

Purity/Quality:

97% ^*data from raw suppliers

3-(1,3-Dioxolan-2-yl)benzophenone 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1COC(O1)C2=CC(=CC=C2)C(=O)C3=CC=CC=C3

Technology Process of 3-(1,3-Dioxolan-2-YL)benzophenone

There total 8 articles about 3-(1,3-Dioxolan-2-YL)benzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide

: 98-88-4
benzoyl chloride

: 85366-46-7
(3-(1,3-dioxolan-2-yl)phenyl)(phenyl)methanone

Guidance literature:: 3-(1,3-dioxolan-2-yl)-phenylbromide; With N,N,N,N,-tetramethylethylenediamine; C₄H₉Mg⁽¹⁺⁾*2C₈H₁₇O^(1-)*Li⁽¹⁺⁾; In toluene; at 25 ℃; for 0.25h; Schlenk technique; Inert atmosphere;

With copper(l) iodide; In toluene; at 0 ℃; for 1h; Schlenk technique; Inert atmosphere;

benzoyl chloride; In toluene; at 0 ℃; for 1h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201802123

Reference yield: 62.0%

: 17789-14-9
3-(1,3-dioxolan-2-yl)-phenylbromide

: 100-52-7
benzaldehyde

: 85366-46-7
(3-(1,3-dioxolan-2-yl)phenyl)(phenyl)methanone

Guidance literature:: 3-(1,3-dioxolan-2-yl)-phenylbromide; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 0.666667h;

benzaldehyde; In tetrahydrofuran; at -78 ℃; for 2h;
DOI:10.1016/j.bmc.2018.03.005