2-Furancarboxylic acid, 2-[6-aMino-1-(2-hydroxyethyl)-1H-pyrazolo[3,4-d]pyriMidin-4-yl]hydrazide

Base Information

Chemical Name:2-Furancarboxylic acid, 2-[6-aMino-1-(2-hydroxyethyl)-1H-pyrazolo[3,4-d]pyriMidin-4-yl]hydrazide
CAS No.:377729-86-7
Molecular Formula:C₁₂H₁₃N₇O₃
Molecular Weight:303.28
Hs Code.:

Synonyms:2-Furancarboxylic acid, 2-[6-aMino-1-(2-hydroxyethyl)-1H-pyrazolo[3,4-d]pyriMidin-4-yl]hydrazide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Furancarboxylic acid, 2-[6-aMino-1-(2-hydroxyethyl)-1H-pyrazolo[3,4-d]pyriMidin-4-yl]hydrazide

Chemical Property:

Purity/Quality:: ≥95% ^*data from raw suppliers

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Technology Process of 2-Furancarboxylic acid, 2-[6-aMino-1-(2-hydroxyethyl)-1H-pyrazolo[3,4-d]pyriMidin-4-yl]hydrazide

There total 3 articles about 2-Furancarboxylic acid, 2-[6-aMino-1-(2-hydroxyethyl)-1H-pyrazolo[3,4-d]pyriMidin-4-yl]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 109-84-2
2-hydroxyethylhydrazine

: 377729-80-1
furan-2-carboxylic acid N-(2-amino-6-chloro-5-formylpyrimidin-4-yl)-hydrazide

: 377729-86-7
C₁₂H₁₃N₇O₃

Guidance literature:: 2-hydroxyethylhydrazine; furan-2-carboxylic acid N-(2-amino-6-chloro-5-formylpyrimidin-4-yl)-hydrazide; In water; at 80 ℃; for 2.5h;

With hydrogenchloride; at 25 ℃; for 2h;

Reference yield:

: 5604-46-6
2-amino-4,6-dichloropyrimidine-5-carboxaldehyde

: 377729-86-7
C₁₂H₁₃N₇O₃

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / 70 °C

2: acetonitrile; water / 2.5 h / Reflux

With triethylamine; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/acs.jmedchem.9b01856

Reference yield:

: 3326-71-4
2-furoic acid hydrazide

: 377729-86-7
C₁₂H₁₃N₇O₃

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 3 h / 70 °C

2: acetonitrile; water / 2.5 h / Reflux

With triethylamine; In tetrahydrofuran; water; acetonitrile;
DOI:10.1021/acs.jmedchem.9b01856