1,3-Dimethylimidazolium bicarbonate

Base Information

• Chemical Name: 1,3-Dimethylimidazolium bicarbonate
• CAS No.: 945017-57-2
• Molecular Formula: CHO₃*C₅H₉N₂
• Molecular Weight: 158.157
• Mol file: 945017-57-2.mol

Synonyms:1,3-Dimethylimidazolium bicarbonate;1,3-Dimethylimidazolium hydrogen carbonate solution

Chemical Property of 1,3-Dimethylimidazolium bicarbonate

Chemical Property:

• Refractive Index: n20/D 1.418
• Flash Point: 57 °C
• PSA: 69.17000
• LogP: -1.26270

Purity/Quality:

97% ^*data from raw suppliers

1,3-DIMETHYLIMIDAZOLIUM HYDROGEN CARBONATE SOLUTION 95.00% ^*data from reagent suppliers

Safty Information:

• Hazard Codes: T
• Statements: 20/21/22-36/37/38-39/23/24/25
• Safety Statements: 26-36/37-45

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-Dimethylimidazolium bicarbonate

There total 5 articles about 1,3-Dimethylimidazolium bicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N,N'-dimethylimidazolium-2-carboxylate (536755-29-0) → 1,3-dimethyl-1H-imidazol-3-ium hydrogen carbonate (945017-57-2)

Guidance literature:

In water; acetonitrile; at 20 ℃; for 24h;

DOI:10.1002/anie.201713079

Reference yield: 85.0%

1,3-dimethylimidazolium chloride (79917-88-7) + potassium carbonate (584-08-7) → 1,3-dimethyl-1H-imidazol-3-ium hydrogen carbonate (945017-57-2)

Guidance literature:

In methanol; at 20 ℃; for 6h;

DOI:10.1016/j.apcata.2011.07.016

Reference yield: 77.0%

carbon dioxide (124-38-9,18923-20-1) + 1,3-dimethylimidazolim iodide (4333-62-4) → 1,3-dimethyl-1H-imidazol-3-ium hydrogen carbonate (945017-57-2) + N,N'-dimethylimidazolium-2-carboxylate (536755-29-0)

Guidance literature:

In N,N-dimethyl-formamide; at 20 ℃; under 760.051 Torr; Overall yield = 99.4 mg; Electrolysis;

DOI:10.1021/ol401949f

upstream raw materials:

carbonic-acid

N,N'-dimethylimidazolium-2-carboxylate

1,3-dimethylimidazolium chloride

potassium carbonate

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