Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI)

Base Information

Chemical Name:Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI)
CAS No.:402937-69-3
Molecular Formula:C8H8ClNO3
Molecular Weight:201.609
Hs Code.:
Mol file:402937-69-3.mol

Synonyms:Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI)

Suppliers and Price of Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI)

Chemical Property:

PSA：66.05000
LogP:2.39020

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI)

There total 3 articles about Benzenemethanol, alpha-(chloromethyl)-3-nitro-, (alphaS)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4128-31-8,113301-48-7,4128-32-9
rac-octan-2-ol

: 99-47-8
2-chloro-1-(3-nitrophenyl)ethanone

: 6169-06-8,113301-48-7,4128-32-9
(S)-2-Octanol

: 402937-69-3,329348-23-4
(S)-2-chloro-1-(3-nitrophenyl)ethanol

Guidance literature:: With Tris-HCl buffer; at 30 ℃; for 24h; pH=7.5; enantioselective reaction; Enzymatic reaction;
DOI:10.1021/jo802350f

Reference yield:

: 99-47-8
2-chloro-1-(3-nitrophenyl)ethanone

: 329348-23-4
(R)-2-chloro-1-(3-nitrophenyl)ethanol

: 402937-69-3,329348-23-4
(S)-2-chloro-1-(3-nitrophenyl)ethanol

Guidance literature:: With glucopyranose; at 30 ℃; for 48h; Overall yield = 21 %; Enzymatic reaction;
DOI:10.1016/j.molcatb.2013.07.021

Reference yield:

: 532-27-4,108321-66-0,164322-25-2
1-chloroacetophenone

: 329348-23-4
(R)-2-chloro-1-(3-nitrophenyl)ethanol

: 402937-69-3,329348-23-4
(S)-2-chloro-1-(3-nitrophenyl)ethanol

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; guanidine nitrate / 30 h / -20 °C

2: glucopyranose / 48 h / 30 °C / Enzymatic reaction

With glucopyranose; sulfuric acid; guanidine nitrate;
DOI:10.1016/j.molcatb.2013.07.021