3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

Base Information

Chemical Name:3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide
CAS No.:6137-38-8
Molecular Formula:C13H8Cl3NO2
Molecular Weight:316.5671
Hs Code.:
DSSTox Substance ID:DTXSID00210288
Wikidata:Q83084945
ChEMBL ID:CHEMBL1814051

Synonyms:3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide;Benzamide, 3,5-dichloro-N-(3-chlorophenyl)-2-hydroxy-;6137-38-8;CHEMBL1814051;SCHEMBL8672680;DTXSID00210288;BDBM50350106

Suppliers and Price of 3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

Chemical Property:

Vapor Pressure:2.18E-06mmHg at 25°C
Boiling Point:382.2°Cat760mmHg
Flash Point:185°C
Density:1.562g/cm³
XLogP3:4.8
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:314.962062
Heavy Atom Count:19
Complexity:329

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)Cl)NC(=O)C2=C(C(=CC(=C2)Cl)Cl)O

Technology Process of 3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

There total 4 articles about 3,5-Dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 320-72-9
3,5-dichlorosalicylic acid

: 108-42-9
3-chloro-aniline

: 6137-38-8
3,5-dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

Guidance literature:: With phosphorus trichloride; In chlorobenzene; for 3h; Heating;
DOI:10.1002/(SICI)1521-4184(199801)331:1<3::AID-ARDP3>3.0.CO;2-2

Reference yield: 62.0%

: 39614-80-7
3,5-dichloro-2-hydroxy-benzoyl chloride

: 108-42-9
3-chloro-aniline

: 6137-38-8
3,5-dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

Guidance literature:: In dichloromethane; at 20 ℃; for 0.5h;
DOI:10.1021/jm200325s

Reference yield:

: 320-72-9
3,5-dichlorosalicylic acid

: 6137-38-8
3,5-dichloro-N-(3-chlorophenyl)-2-hydroxybenzamide

Guidance literature:: Multi-step reaction with 2 steps

1: thionyl chloride / 110 °C

2: dichloromethane / 0.5 h / 20 °C

With thionyl chloride; In dichloromethane;
DOI:10.1021/jm200325s