[4aS,8aR,(+)]-Decahydroquinazoline

Base Information

Chemical Name:[4aS,8aR,(+)]-Decahydroquinazoline
CAS No.:26685-89-2
Molecular Formula:C₈H₁₆N₂
Molecular Weight:140.228
Hs Code.:
Mol file:26685-89-2.mol

Synonyms:[4aS,8aR,(+)]-Decahydroquinazoline

Suppliers and Price of [4aS,8aR,(+)]-Decahydroquinazoline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of [4aS,8aR,(+)]-Decahydroquinazoline

Chemical Property:

Boiling Point:197.6±8.0 °C(Predicted)
PKA:10.25±0.20(Predicted)
Density:0.931±0.06 g/cm3(Predicted)

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [4aS,8aR,(+)]-Decahydroquinazoline

There total 8 articles about [4aS,8aR,(+)]-Decahydroquinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 22.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 24716-89-0,24716-96-9,24717-04-2,26685-87-0,26853-49-6,26853-51-0,40015-92-7,75197-09-0,75197-10-3
cis-2-amino-1-aminomethylcyclohexane

: 24716-87-8,24717-09-7,26685-89-2,26693-40-3,26693-41-4,45761-20-4,61557-94-6
cis-decahydroquinazoline

Guidance literature:: In water;
DOI:10.1016/S0040-4020(01)85926-3

Reference yield:

: 1469-49-4,2028-12-8
6-carbamoylcyclohex-3-enecarboxylic acid

: 24716-87-8,24717-09-7,26685-89-2,26693-40-3,26693-41-4,45761-20-4,61557-94-6
cis-decahydroquinazoline

Guidance literature:: Multi-step reaction with 5 steps

1: 91 percent / H₂ / 10percent Pt/C / ethanol / 760 Torr / Ambient temperature

2: 1.) bromine, NaOH; 2.) HCl / 1.) water, 75 deg C, 2 min; 2.) reflux, 3 h

3: 66 percent

4: 38 percent / lithium aluminium hydride / diethyl ether

5: 22 percent / H₂O

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; bromine; platinum on activated charcoal; In diethyl ether; ethanol; water;
DOI:10.1016/S0040-4020(01)85926-3

Reference yield:

: 1436-60-8,1436-61-9,24716-94-7,26849-62-7,64162-07-8,75197-07-8,115014-75-0
ethyl cis-2-amino-1-cyclohexanecarboxylate

: 24716-87-8,24717-09-7,26685-89-2,26693-40-3,26693-41-4,45761-20-4,61557-94-6
cis-decahydroquinazoline

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent

2: 38 percent / lithium aluminium hydride / diethyl ether

3: 22 percent / H₂O

With lithium aluminium tetrahydride; In diethyl ether; water;
DOI:10.1016/S0040-4020(01)85926-3