Technology Process of N-(tert-butyl)-N-(2-chlorobenzyl)amine
There total 3 articles about N-(tert-butyl)-N-(2-chlorobenzyl)amine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
C13H20BCl2N2(1+)*C24BF20(1-); hydrogen;
In
dichloromethane;
at 20 ℃;
for 0.5h;
under 77525.2 Torr;
DOI:10.1039/c4sc03675a
- Guidance literature:
-
2-chloro-benzaldehyde; tert-butylamine;
In
methanol;
at 20 ℃;
for 3h;
With
sodium tetrahydroborate;
In
methanol;
for 1h;
DOI:10.1016/j.tet.2017.06.029
- Guidance literature:
-
Multi-step reaction with 2 steps
1: toluene / 10 h / Reflux
2: sodium tetrahydroborate / tetrahydrofuran; methanol / 18 h / 20 °C
With
sodium tetrahydroborate;
In
tetrahydrofuran; methanol; toluene;
DOI:10.1039/c1ob05618b