9(10H)-Acridinone, 1-nitro-

Base Information

• Chemical Name: 9(10H)-Acridinone, 1-nitro-
• CAS No.: 40239-75-6
• Molecular Formula: C₁₃H₈N₂O₃
• Molecular Weight: 240.218
• NSC Number: 170668
• UNII: K26TEP6QBV
• DSSTox Substance ID: DTXSID00193224
• Nikkaji Number: J531.546H
• Wikidata: Q83065932
• Mol file: 40239-75-6.mol

Synonyms:1-Nitroacridone;9(10H)-Acridinone, 1-nitro-;1-Nitro-9(10H)-acridinone;K26TEP6QBV;40239-75-6;NSC 170668;BRN 0216836;NSC-170668;5-21-09-00015 (Beilstein Handbook Reference);1-nitro-10H-acridin-9-one;nitroacridone;NSC170668;1-nitro-9-acridanone;UNII-K26TEP6QBV;1-nitroacridin-9(10H)-one;SCHEMBL5142127;DTXSID00193224

Chemical Property of 9(10H)-Acridinone, 1-nitro-

Chemical Property:

• Vapor Pressure: 1.25E-07mmHg at 25°C
• Boiling Point: 430.9°Cat760mmHg
• Flash Point: 214.4°C
• Density: 1.409g/cm³
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 0
• Exact Mass: 240.05349212
• Heavy Atom Count: 18
• Complexity: 366

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C2C(=C1)C(=O)C3=C(N2)C=CC=C3[N+](=O)[O-]

Technology Process of 9(10H)-Acridinone, 1-nitro-

There total 23 articles about 9(10H)-Acridinone, 1-nitro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-nitro-9-acridanone (40239-75-6) + 3-nitro-9,10-dihydroacridin-9-one (1744-92-9)

Guidance literature:

With sulfuric acid;

DOI:10.1039/jr9460000102

Reference yield:

2-(3-nitrophenylamino)-benzoyl chloride → 1-nitro-9-acridanone (40239-75-6)

Guidance literature:

With hydrogenchloride; In water; for 2h; Heating;

DOI:10.1016/j.jphotobiol.2016.05.028

Reference yield:

potassium 2-bromo-4-acetylaminobenzoate (86026-76-8) → 1-nitro-9-acridanone (40239-75-6)

Guidance literature:

Multi-step reaction with 5 steps

1: 54 percent / Cu powder / 0.5 h / 160 °C

2: 1.) POCl₃ / 1.) reflux, 1 h, 2.) 50 deg C, 40 min

3: 1.) phenol / 1.) 80 deg C, 15 min, 2.) 60 deg C, 20 min

4: 1.7 g / 36percent aq. H₂SO₄ / ethanol / 8 h / Heating

5: H₂SO₄, NaNO₂ / aq. ethanol / 1.) 10 deg C, 20 min, 2.) heating

With sulfuric acid; sodium nitrite; trichlorophosphate; phenol; copper; In ethanol;

upstream raw materials:

1-Nitroacridine

1-nitro-9-chloroacridine

N-(3-nitrophenyl)anthranilic acid

6-amino-1-nitroacridone

Downstream raw materials:

acridin-1-ylamine

1-nitro-9-chloroacridine

1-aminoacridin-9(10H)-one

1-hydroxylamino-9-acridone