4-METHOXY-3-MORPHOLIN-4-YLMETHYL-BENZALDEHYDE

Base Information

• Chemical Name: 4-METHOXY-3-MORPHOLIN-4-YLMETHYL-BENZALDEHYDE
• CAS No.: 128501-81-5
• Molecular Formula: C13H17NO3
• Molecular Weight: 235.283
• Mol file: 128501-81-5.mol

Synonyms:ART-CHEM-BB B000991;AKOS B000991;4-METHOXY-3-(4-MORPHOLINYLMETHYL)BENZALDEHYDE;4-METHOXY-3-MORPHOLIN-4-YLMETHYL-BENZALDEHYDE;TIMTEC-BB SBB000738;4-Methoxy-3-(morpholinomethyl)benzaldehyde

Chemical Property of 4-METHOXY-3-MORPHOLIN-4-YLMETHYL-BENZALDEHYDE

Chemical Property:

• PSA: 38.77000
• LogP: 1.27780

Purity/Quality:

97% ^*data from raw suppliers

4-Methoxy-3-(morpholin-4-ylmethyl)benzaldehyde ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

Useful:

• Uses: 4-Methoxy-3-(morpholin-4-ylmethyl)benzaldehyde is used in the synthesis of 2-Aryl 1,2-Dihydro-4(3H)-quinazoline derivative possessing anticancer and antiparasitic activities and capable of preventing the progress of neurodegenerative diseases.

Technology Process of 4-METHOXY-3-MORPHOLIN-4-YLMETHYL-BENZALDEHYDE

There total 2 articles about 4-METHOXY-3-MORPHOLIN-4-YLMETHYL-BENZALDEHYDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

morpholine (110-91-8,99108-56-2) + 3-(chloromethyl)-4-methoxybenzaldehyde (52577-09-0) → 4-methoxy-3-(morpholinomethyl)benzaldehyde (128501-81-5)

Guidance literature:

With potassium carbonate; In ethanol; Reflux;

DOI:10.1007/s11172-015-0875-9

Reference yield:

4-methoxy-benzaldehyde (123-11-5) → 4-methoxy-3-(morpholinomethyl)benzaldehyde (128501-81-5)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrogenchloride / water / 3 h / 70 - 80 °C

2: potassium carbonate / ethanol / Reflux

With hydrogenchloride; potassium carbonate; In ethanol; water;

DOI:10.1007/s11172-015-0875-9

Reference yield: 88.0%

4-methoxy-3-(morpholinomethyl)benzaldehyde (128501-81-5) + 2-amino-N-(4'-fluorophenyl)benzamide (216502-06-6) → C26H26FN3O3*ClH

Guidance literature:

4-methoxy-3-(morpholinomethyl)benzaldehyde; 2-amino-N-(4-fluorophenyl)benzamide; With acetic acid; In 5,5-dimethyl-1,3-cyclohexadiene; Reflux;

With hydrogenchloride; In water;

DOI:10.1007/s11172-017-1852-2

upstream raw materials:

morpholine

3-(chloromethyl)-4-methoxybenzaldehyde

4-methoxy-benzaldehyde

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