3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)-2-Pyridinamine

Base Information

Chemical Name:3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)-2-Pyridinamine
CAS No.:1174046-75-3
Molecular Formula:C₂₄H₁₅ClFN₃O₃
Molecular Weight:447.853
Hs Code.:
Mol file:1174046-75-3.mol

Synonyms:3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)-2-Pyridinamine

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Chemical Property of 3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)-2-Pyridinamine

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Technology Process of 3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)-2-Pyridinamine

There total 4 articles about 3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)-2-Pyridinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1174046-74-2
3-chloro-2-((diphenylmethylene)amino)pyridin-4(1H)-one

: 369-34-6
3,4-difluoronitrobenzene

: 1174046-75-3
3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)pyridin-2-amine

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 1h; Large scale;
DOI:10.1021/op3002239

Reference yield:

: 2402-77-9
2,3-dichloro-pyridine

: 1174046-75-3
3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)pyridin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / 2-methyltetrahydrofuran / 18 h / 80 °C / Large scale

2: sodium percarbonate; lithium diisopropyl amide; triisopropylborane / water / 3 h / 0 - 25 °C / Large scale

3: caesium carbonate / N,N-dimethyl-formamide / 1 h / 90 °C / Large scale

With sodium percarbonate; triisopropylborane; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; lithium diisopropyl amide; In 2-methyltetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/op3002239

Reference yield:

: benzophenoneimine

: 1174046-75-3
3-chloro-N-(diphenylmethylene)-4-(2-fluoro-4-nitrophenoxy)pyridin-2-amine

Guidance literature:: Multi-step reaction with 3 steps

1: palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; caesium carbonate / 2-methyltetrahydrofuran / 18 h / 80 °C / Large scale

2: sodium percarbonate; lithium diisopropyl amide; triisopropylborane / water / 3 h / 0 - 25 °C / Large scale

3: caesium carbonate / N,N-dimethyl-formamide / 1 h / 90 °C / Large scale

With sodium percarbonate; triisopropylborane; palladium diacetate; caesium carbonate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; lithium diisopropyl amide; In 2-methyltetrahydrofuran; water; N,N-dimethyl-formamide;
DOI:10.1021/op3002239