1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Base Information

Chemical Name:1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-
CAS No.:943324-08-1
Molecular Formula:C20H23BN2O4S
Molecular Weight:398.291
Hs Code.:2933990090
Mol file:943324-08-1.mol

Synonyms:1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-;2-Methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetraMethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine;2-Methyl-1-(phenylsulfonyl)-1H-Pyrrolo[2,3-b]pyridine-3-boronic acid pinacol ester

Suppliers and Price of 1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Synthonix
2-Methyl-1-(phenylsulfonyl)-1H-Pyrrolo[2,3-b]pyridine-3-boronicacidpinacolester 97.0%
250mg
$ 390.00

SynQuest Laboratories
2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine-3-boronic acid, pinacol ester
250 mg
$ 475.00

Matrix Scientific
2-Methyl-1-(phenylsulfonyl)-1H-pyrrolo[2,3-b]pyridine-3-boronic acid pinacol ester
1g
$ 1796.00

Crysdot
2-Methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine 95+%
1g
$ 1280.00

Chemenu
2-Methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine 95%+
250mg
$ 747.00

Chemenu
2-Methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine 95%+
1g
$ 2115.00

Alichem
2-Methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine
1g
$ 1331.20

Total 16 raw suppliers

Chemical Property of 1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

Chemical Property:

Vapor Pressure:2.43E-13mmHg at 25°C
Boiling Point:577.6°C at 760 mmHg
Flash Point:303.1°C
PSA：78.80000
Density:1.24g/cm³
LogP:3.96170

Purity/Quality:

99%, ^*data from raw suppliers

2-Methyl-1-(phenylsulfonyl)-1H-Pyrrolo[2,3-b]pyridine-3-boronicacidpinacolester 97.0% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-

There total 4 articles about 1H-Pyrrolo[2,3-b]pyridine, 2-methyl-1-(phenylsulfonyl)-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943324-07-0
3-Iodo-2-methyl-1-(phenylsulfonyl)pyrrolo[2,3-b]pyridine

: 73183-34-3
bis(pinacol)diborane

: 943324-08-1
1-benzenesulfonyl-2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: With potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; In N,N-dimethyl-formamide; at 90 ℃; for 12h;

Reference yield:

: 73183-34-3
bis(pinacol)diborane

: 744209-37-8
3-bromo-2-methyl-1-phenylsulfonylpyrrolo[2,3-b]pyridine

: 943324-08-1
1-benzenesulfonyl-2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; potassium acetate; In diethylene glycol dimethyl ether; at 120 ℃; for 3h;

Reference yield:

: 143141-23-5
1-benzenesulfonyl-1H-pyrrolo[2,3-b]pyridine

: 943324-08-1
1-benzenesulfonyl-2-methyl-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1H-pyrrolo[2,3-b]pyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium diisopropyl amide / tetrahydrofuran; n-heptane / 0.83 h / -70 - 20 °C / Inert atmosphere

1.2: 15 h / -70 - 20 °C

2.1: N-Bromosuccinimide / N,N-dimethyl-formamide / 1 h / 20 °C

3.1: bis-triphenylphosphine-palladium(II) chloride; potassium acetate / diethylene glycol dimethyl ether / 3 h / 120 °C

With bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; potassium acetate; lithium diisopropyl amide; In tetrahydrofuran; n-heptane; diethylene glycol dimethyl ether; N,N-dimethyl-formamide;