2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Base Information

Chemical Name:2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane
CAS No.:1437053-63-8
Molecular Formula:C₁₉H₃₁BO₄
Molecular Weight:0
Hs Code.:
Mol file:1437053-63-8.mol

Synonyms:2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Chemical Property of 2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

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Technology Process of 2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

There total 1 articles about 2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1437053-60-5
2-bromo-1-(2-(ethoxymethoxy)propan-2-yl)-4-methylbenzene

: 73183-34-3
bis(pinacol)diborane

: 1437053-63-8
2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In 1,4-dioxane; at 80 ℃; Inert atmosphere;

Reference yield:

: 1437053-63-8
2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1437050-72-0
5-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)-N-((1-hydroxy-3,3-dimethyl-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)methyl)-N-methylindolizine-8-carboxamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / tetrahydrofuran / 20 °C

2: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 16 h / 20 °C / Reflux

3: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 °C / pH 6

4: HATU; triethylamine

With hydrogenchloride; N-Bromosuccinimide; sodium tris(acetoxy)borohydride; acetic acid; triethylamine; HATU; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane;

Reference yield:

: 1437053-63-8
2-(2-(2-(ethoxymethoxy)propan-2-yl)-5-methylphenyl)-4,4,5,5-tetramethyl-1,3,2-dioxaborolane

: 1437049-39-2
4-(5-(3,5-dichlorophenyl)-5-(trifluoromethyl)-4,5-dihydroisoxazol-3-yl)-N-((1-hydroxy-3,3-dimethyl-1,3-dihydrobenzo[c][1,2]oxaborol-6-yl)methyl)-N,2-dimethylbenzamide

Guidance literature:: Multi-step reaction with 4 steps

1: hydrogenchloride / tetrahydrofuran / 20 °C

2: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 16 h / 20 °C / Reflux

3: acetic acid; sodium tris(acetoxy)borohydride / tetrahydrofuran / 20 °C / pH 6

4: 2-bromo-1-ethylpyridin-1-ium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

With hydrogenchloride; N-Bromosuccinimide; sodium tris(acetoxy)borohydride; 2-bromo-1-ethylpyridin-1-ium tetrafluoroborate; acetic acid; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; dichloromethane;