(3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3β,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione

Base Information

Chemical Name:(3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3β,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione
CAS No.:17956-11-5
Molecular Formula:C15H22O3
Molecular Weight:250.338
Hs Code.:
Mol file:17956-11-5.mol

Synonyms:(3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione;(3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3β,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione;β-Tetrahydrosantonin;β-Tetrahydro-α-santonin

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3β,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione

Chemical Property:

PSA：43.37000
LogP:2.57940

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3β,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione

There total 12 articles about (3S)-3aβ,5,5a,6,7,9,9aα,9bα-Octahydro-3β,5aα,9α-trimethylnaphtho[1,2-b]furan-2,8(3H,4H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 481-07-2
β-santonin

: 13902-54-0,13902-55-1,13902-61-9,14794-68-4,14804-46-7,14804-47-8,14987-66-7,17956-11-5,18409-87-5,32638-47-4,84652-34-6,143521-75-9,143521-76-0
(11R)-6α-hydroxy-3-oxo-4βH,5β-eudesman-12-oic acid-lactone

: 32638-47-4
(11R)-6α-hydroxy-3-oxo-5β-eudesman-12-oic acid-lactone

Guidance literature:: With potassium hydroxide; anschliessend Hydrieren an Raney-Nickel und Erwaermen des Reaktionsprodukts mit wss. Salzsaeure;
DOI:10.1021/jo01103a008

Reference yield:

: 13902-54-0,13902-55-1,13902-61-9,14794-68-4,14804-46-7,14804-47-8,14987-66-7,17956-11-5,18409-87-5,32638-47-4,84652-34-6,143521-75-9,143521-76-0
tetrahydrosantonin

Guidance literature:: Santonin, H2/Pd-C/A.;
DOI:10.1021/ja00888a015

Reference yield:

: 13902-54-0,13902-55-1,13902-61-9,14794-68-4,14804-46-7,14804-47-8,14987-66-7,17956-11-5,18409-87-5,32638-47-4,84652-34-6,143521-75-9,143521-76-0
Tetrahydro-santonin C

Guidance literature:: Aus (-)-Santonin C, H2/Pd-C/Eg. (Raumt., Normaldruck); daneben 1ζ-Methyl-2-oxo-4ar,7c-(1-carboxy-ethyl)-8aζ(H)-decalin;
DOI:10.1021/ja01494a036