3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane

Base Information

Chemical Name:3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane
CAS No.:478696-46-7
Molecular Formula:C15H19N3
Molecular Weight:241.336
Hs Code.:
Mol file:478696-46-7.mol

Synonyms:3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane

Suppliers and Price of 3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane

Chemical Property:

PSA：29.85000
LogP:3.12900

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

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Technology Process of 3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane

There total 2 articles about 3-(2-Methyl-1H-benzo[d]iMidazol-1-yl)-8-aza-bicyclo[3.2.1]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 280762-13-2
endo-tert-butyl 3-[(2-aminophenyl)amino]-8-azabicyclo[3.2.1]octane-8-carboxylate

: 78-39-7
Triethyl orthoacetate

: 478696-46-7
endo-1-(8-azabicyclo[3.2.1]oct-3-yl)-2-methyl-1H-benzimidazole

Guidance literature:: for 2.5h; Inert atmosphere; Reflux;
DOI:10.1021/jm800598a

Reference yield:

: 1-(8-benzyl-8-azabicyclo[3.2.1]oct-3-yl)-2-methyl-1H-benzimidazole

: 478696-46-7
endo-1-(8-azabicyclo[3.2.1]oct-3-yl)-2-methyl-1H-benzimidazole

Guidance literature:: With ammonium formate; palladium(II) hydroxide/carbon; In ethanol; for 2.5h; Heating / reflux;

Reference yield: 99.0%

: 716358-39-3
tert-butyl 4-(3-chlorophenyl)-4-(2-oxoethyl)piperidine-1-carboxylate

: 478696-46-7
endo-1-(8-azabicyclo[3.2.1]oct-3-yl)-2-methyl-1H-benzimidazole

: 716358-40-6
tert-butyl endo-4-(3-chlorophenyl)-4-{2-[3-(2-methyl-1H-benzimidazol-1-yl)-8-azabicyclo[3.2.1]oct-8-yl]ethyl}piperidine-1-carboxylate

Guidance literature:: With sodium tris(acetoxy)borohydride; triethylamine; In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Molecular sieve;
DOI:10.1021/jm800598a