4-BUTYLTHIOPHENYLBORONIC ACID

Base Information

• Chemical Name: 4-BUTYLTHIOPHENYLBORONIC ACID
• CAS No.: 151588-38-4
• Molecular Formula: C₁₀H₁₅BO₂S
• Molecular Weight: 210.105
• Hs Code.: 2931900090
• Mol file: 151588-38-4.mol

Synonyms:4-BUTYLSULFANYLPHENYLBORONIC ACID;4-BUTYLTHIOPHENYLBORONIC ACID;AKOS BRN-0642

Chemical Property of 4-BUTYLTHIOPHENYLBORONIC ACID

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Boiling Point: 366.628°C at 760 mmHg
• Flash Point: 175.531°C
• PSA: 65.76000
• Density: 1.126g/cm³
• LogP: 1.25860

Purity/Quality:

97% ^*data from raw suppliers

4-Butylthiophenylboronic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-BUTYLTHIOPHENYLBORONIC ACID

There total 1 articles about 4-BUTYLTHIOPHENYLBORONIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Trimethyl borate (121-43-7,63156-11-6) + 1-Bromo-4-butylsulphanylbenzene (121392-35-6) → (4-(butylthio)phenyl)boronic acid (151588-38-4)

Guidance literature:

With n-butyllithium;

DOI:10.1002/adfm.201702318

Reference yield: 69.0%

ethyl 2-(3-(4-((4'-hydroxy-2',6'-dimethyl-[1,1'-biphenyl]-3-yl)methoxy)phenyl)oxetan-3-yl)acetate (1453861-34-1) + (4-(butylthio)phenyl)boronic acid (151588-38-4) → ethyl 2-(3-(4-((4'-(butylthio)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)oxetan-3-yl)acetate (1453861-79-4)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,4-dioxane; water; at 120 ℃; for 0.166667h; Inert atmosphere; Microwave irradiation;

upstream raw materials:

Trimethyl borate

1-Bromo-4-butylsulphanylbenzene

Downstream raw materials:

ethyl 2-(3-(4-((4'-(butylthio)-[1,1'-biphenyl]-3-yl)methoxy)phenyl)oxetan-3-yl)acetate

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