Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy-

Base Information

Chemical Name:Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy-
CAS No.:166115-79-3
Molecular Formula:C₁₄H₁₆N₄O₄
Molecular Weight:304.305
Hs Code.:
Mol file:166115-79-3.mol

Synonyms:Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy-

Suppliers and Price of Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy-

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Technology Process of Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy-

There total 2 articles about Acetamide, N-(6-amino-1,2,3,4-tetrahydro-1,3-dimethyl-2,4-dioxo-5-pyrimidinyl)-2-phenoxy- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 5440-00-6
4,5-Diamino-1,3-dimethyluracil

: 701-99-5
Phenoxyacetyl chloride

: 166115-79-3
N-(6-Amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl)-2-phenoxy-acetamide

Guidance literature:: With pyridine; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1016/0223-5234(96)88233-X

Reference yield:

: 5440-00-6
4,5-Diamino-1,3-dimethyluracil

: 122-59-8
2-phenoxyacetic acid

: 166115-79-3
N-(6-Amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl)-2-phenoxy-acetamide

Guidance literature:: With N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In 1,4-dioxane; water; at 20 ℃;
DOI:10.1016/j.bmc.2015.09.012

Reference yield:

: 166115-79-3
N-(6-Amino-1,3-dimethyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidin-5-yl)-2-phenoxy-acetamide

: 1388725-76-5
8-(phenoxymethyl)-1,3,7-trimethylxanthine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / water / Reflux

2: potassium carbonate / acetone

With potassium carbonate; sodium hydroxide; In water; acetone;
DOI:10.1016/j.bmc.2015.09.012