4-BroMo-3-chloro-N-Methyl-2-nitroanilin

Base Information

Chemical Name:4-BroMo-3-chloro-N-Methyl-2-nitroanilin
CAS No.:1357159-31-9
Molecular Formula:C7H6BrClN2O2
Molecular Weight:265.494
Hs Code.:

Synonyms:4-BroMo-3-chloro-N-Methyl-2-nitroanilin;Benzenamine, 4-bromo-3-chloro-N-methyl-2-nitro-;4-Bromo-3-chloro-N-methyl-2-nitroaniline

Suppliers and Price of 4-BroMo-3-chloro-N-Methyl-2-nitroanilin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
4-Bromo-3-chloro-N-methyl-2-nitroaniline 95%
10g
$ 2036.00

Matrix Scientific
4-Bromo-3-chloro-N-methyl-2-nitroaniline 95%
5g
$ 1573.00

Crysdot
4-Bromo-3-chloro-N-methyl-2-nitroaniline 97%
1g
$ 1135.00

Crysdot
4-Bromo-3-chloro-N-methyl-2-nitroaniline 97%
5g
$ 2845.00

Alichem
4-Bromo-3-chloro-n-methyl-2-nitroaniline
10g
$ 4411.33

Aaron Chemicals
4-Bromo-3-chloro-N-methyl-2-nitroaniline 95%
1g
$ 957.00

Aaron Chemicals
4-Bromo-3-chloro-N-methyl-2-nitroaniline 95%
250mg
$ 482.00

Aaron Chemicals
4-Bromo-3-chloro-N-methyl-2-nitroaniline 95%
100mg
$ 292.00

Total 3 raw suppliers

Chemical Property of 4-BroMo-3-chloro-N-Methyl-2-nitroanilin

Chemical Property:

PSA：57.85000
LogP:3.64860

Purity/Quality:

95% purity ^*data from raw suppliers

4-Bromo-3-chloro-N-methyl-2-nitroaniline 95% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 4-BroMo-3-chloro-N-Methyl-2-nitroanilin

There total 4 articles about 4-BroMo-3-chloro-N-Methyl-2-nitroanilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.8%

: 1000573-99-8
4-bromo-3-chloro-2-nitro aniline

: 74-88-4
methyl iodide

: 1357159-31-9
4-bromo-3-chloro-N-methyl-2-nitroaniline

Guidance literature:: 4-bromo-3-chloro-2-nitro aniline; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

methyl iodide; In N,N-dimethyl-formamide; for 0.5h;

Reference yield: 42.0%

: 1000573-99-8
4-bromo-3-chloro-2-nitro aniline

: 77-78-1
dimethyl sulfate

: 1357159-31-9
4-bromo-3-chloro-N-methyl-2-nitroaniline

Guidance literature:: 4-bromo-3-chloro-2-nitro aniline; With trifluoroacetic anhydride; In toluene; at 0 ℃; for 0.166667h; Inert atmosphere;

dimethyl sulfate; With N-benzyl-N,N,N-triethylammonium chloride; sodium hydroxide; In water; toluene; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/jm201394e

Reference yield:

: 59483-54-4
3-chloro-2-nitro-aniline

: 1357159-31-9
4-bromo-3-chloro-N-methyl-2-nitroaniline

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid; N-Bromosuccinimide / 0.75 h / Reflux

2.1: sodium hydride / N,N-dimethyl-formamide / 0.5 h / 0 °C

2.2: 0.5 h

With N-Bromosuccinimide; sodium hydride; acetic acid; In N,N-dimethyl-formamide;