MethanesulfonaMide, N-Methyl-N-4-piperidinyl-

Base Information

• Chemical Name: MethanesulfonaMide, N-Methyl-N-4-piperidinyl-
• CAS No.: 70724-74-2
• Molecular Formula: C7H16N2O2S
• Molecular Weight: 192.27914
• Hs Code.: 2935009090
• Mol file: 70724-74-2.mol

Synonyms:MethanesulfonaMide, N-Methyl-N-4-piperidinyl-;N-Methyl-N-4-piperidinyl-methanesulfonamide;N-Methyl-N-(piperidin-4-yl)MethanesulfonaMide;N-Methyl-N-(4-piperidyl)methanesulfonamide

Chemical Property of MethanesulfonaMide, N-Methyl-N-4-piperidinyl-

Chemical Property:

• PSA: 57.79000
• LogP: 1.03940
• Storage Temp.: under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

N-Methyl-N-4-piperidinylmethanesulfonamide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of MethanesulfonaMide, N-Methyl-N-4-piperidinyl-

There total 2 articles about MethanesulfonaMide, N-Methyl-N-4-piperidinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methanesulfonyl chloride (124-63-0) + 4-methylamino-piperidine-1-carboxylic acid tert-butyl ester (147539-41-1) → N-methyl-N-(piperidin-4-yl)methanesulfonamide (70724-74-2)

Guidance literature:

With triethylamine; In dichloromethane; for 3h;

Reference yield:

1-Acetyl-4-methylaminopiperidine (139062-96-7) + methanesulfonyl chloride (124-63-0) → N-methyl-N-(piperidin-4-yl)methanesulfonamide (70724-74-2)

Guidance literature:

With sodium hydroxide; triethylamine; In ethanol; chloroform;

Reference yield:

N-methyl-N-(piperidin-4-yl)methanesulfonamide (70724-74-2) + 2-bromo-1-{(3RS,4SR)-3-(3,4-dichloro-phenyl)-4-[(RS)-1-(4-trifluoromethyl-phenoxy)-ethyl]-pyrrolidin-1-yl}-ethanone → N-[1-(2-{(3RS,4SR)-3-(3,4-dichloro-phenyl)-4-[(RS)-1-(4-trifluoromethyl-phenoxy)-ethyl]-pyrrolidin-1-yl}-2-oxo-ethyl)-piperidin-4-yl]-N-methyl-methanesulfonamide

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

upstream raw materials:

1-Acetyl-4-methylaminopiperidine

methanesulfonyl chloride

4-methylamino-piperidine-1-carboxylic acid tert-butyl ester

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