(S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride

Base Information

• Chemical Name: (S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride
• CAS No.: 123191-59-3
• Molecular Formula: C₁₂H₂₂N₂O₆*ClH
• Molecular Weight: 326.777

Synonyms:(S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride

Chemical Property of (S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride

Chemical Property:

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Technology Process of (S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride

There total 1 articles about (S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-α-(tert-butoxycarbonyl)-L-lysine methyl ester (55757-60-3) → (S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride (123191-59-3)

Guidance literature:

Multi-step reaction with 3 steps

1: pyridine

2: 20percent CF₃COOH / CH₂Cl₂

3: HCl / methanol

With pyridine; hydrogenchloride; trifluoroacetic acid; In methanol; dichloromethane;

DOI:10.1016/S0040-4039(00)95188-8

Reference yield:

(S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride (123191-59-3) → (S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid (94732-87-3)

Guidance literature:

Multi-step reaction with 4 steps

1: NaBH₃CN / methanol

2: KOD / D₂O

3: H₂, pyridine, CH₃COOH / Pd-C / methanol / pH 5.8

With pyridine; potassium deuteroxide; hydrogen; sodium cyanoborohydride; acetic acid; palladium on activated charcoal; In methanol; water-d2;

DOI:10.1016/S0040-4039(00)95188-8

Reference yield:

(S)-2-Amino-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester; hydrochloride (123191-59-3) → (S)-2-{2-[Benzyloxycarbonyl-((R)-1-carboxy-ethyl)-amino]-ethylamino}-6-((S)-3-carboxy-3-hydroxy-propionylamino)-hexanoic acid

Guidance literature:

Multi-step reaction with 2 steps

1: NaBH₃CN / methanol

2: KOD / D₂O

With potassium deuteroxide; sodium cyanoborohydride; In methanol; water-d2;

DOI:10.1016/S0040-4039(00)95188-8

upstream raw materials:

N-α-(tert-butoxycarbonyl)-L-lysine methyl ester

Downstream raw materials:

(S)-2-{2-[Benzyloxycarbonyl-((R)-1-methoxycarbonyl-ethyl)-amino]-ethylamino}-6-((S)-3-hydroxy-3-methoxycarbonyl-propionylamino)-hexanoic acid methyl ester

rhizobactin

(S)-2-[[2-((R)-1-Carboxy-ethylamino)-ethyl]-(2,4-dinitro-phenyl)-amino]-6-[((S)-3-carboxy-3-hydroxy-propionyl)-(2,4-dinitro-phenyl)-amino]-hexanoic acid

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