p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

Base Information

Chemical Name:p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside
CAS No.:1242060-81-6
Molecular Formula:C₂₃H₂₅NO₆S
Molecular Weight:443.521
Hs Code.:

Synonyms:p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

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Technology Process of p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

There total 1 articles about p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 1242060-78-1
p-tolyl 2-acetamido-4,6-O-benzylidene-2,3-N,O-carbonyl-2-deoxy-1-thio-β-D-galactopyranoside

: 1242060-81-6
p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

Guidance literature:: With triethylsilane; trifluorormethanesulfonic acid; In dichloromethane; at -72 ℃; for 1h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2010.05.031

Reference yield: 100.0%

: 1242060-81-6
p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1363497-23-7
para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 70 ℃; for 48h;
DOI:10.1002/chem.201102615

Reference yield:

: 1242060-81-6
p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

: C₂₂H₄₀F₃NO₉SSi₂

: 1242060-87-2
p-tolyl (2-acetamido-4,6-di-O-tert-butyldimethylsilyl-2,3-N,O-carbonyl-2-deoxy-α-D-galactopyranosyl)-(1->4)-2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

Guidance literature:: With 2,4,6-tri-tert-butylpyrimidine; In dichloromethane; at -72 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.carres.2010.05.031