para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

Base Information

Chemical Name:para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside
CAS No.:1363497-23-7
Molecular Formula:C₂₉H₃₉NO₆SSi
Molecular Weight:557.783
Hs Code.:

Synonyms:para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

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Chemical Property of para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

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Technology Process of para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

There total 1 articles about para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1242060-81-6
p-tolyl 2-acetamido-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1363497-23-7
para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 70 ℃; for 48h;
DOI:10.1002/chem.201102615

Reference yield: 85.0%

: 1363497-23-7
para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

: 107-18-6
allyl alcohol

: allyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-α-D-galactopyranoside

Guidance literature:: With p-methylbenzenesulfenyl chloride; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -72 - 20 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1002/chem.201702114

Reference yield: 81.0%

: 1363497-23-7
para-tolyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-1-thio-α-D-galactopyranoside

: 107-19-7
propargyl alcohol

: propargyl 2-acetamido-4-O-tert-butyldimethylsilyl-6-O-benzyl-2,3-N,O-carbonyl-2-deoxy-α-D-galactopyranoside

Guidance literature:: With p-methylbenzenesulfenyl chloride; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -72 - 20 ℃; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201702114