1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

Base Information

Chemical Name:1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea
CAS No.:1135227-75-6
Molecular Formula:C₁₈H₁₈ClN₃O₅S₂
Molecular Weight:455.943
Hs Code.:

Synonyms:1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

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Chemical Property of 1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

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Technology Process of 1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

There total 3 articles about 1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 1595285-55-4
4-(2-(4-chlorophenyl)-2-oxoethylamino)benzenesulfonamide

: 16182-04-0
Ethoxycarbonyl isothiocyanate

: 1135227-75-6
1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

Guidance literature:: In acetonitrile; for 6h; Reflux;
DOI:10.1016/j.bmcl.2014.02.030

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 1135227-75-6
1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 4 h / Reflux

2: acetonitrile / 6 h / Reflux

In methanol; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.030

Reference yield:

: 63-74-1
sulfanilamide

: 1135227-75-6
1-(ethoxycarbonyl)-3-(4-aminosulfonylphenyl)-3-(4-chlorophenacyl)thiourea

Guidance literature:: Multi-step reaction with 2 steps

1: methanol / 4 h / Reflux

2: acetonitrile / 6 h / Reflux

In methanol; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.030