6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal

Base Information

• Chemical Name: 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal
• CAS No.: 1033614-68-4
• Molecular Formula: C₃₁H₃₂N₄O₁₃S₂
• Molecular Weight: 732.746

Synonyms:6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal

Chemical Property of 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal

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Technology Process of 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal

There total 1 articles about 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

3-deoxy-3-(N-nosylamino)-D-gulal (1033614-66-2) + C20H22N2O9S2 (1033614-70-8) → 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal (1033614-68-4)

Guidance literature:

With potassium carbonate; In acetonitrile; at 20 ℃; for 16h; stereoselective reaction; Inert atmosphere;

DOI:10.1021/ol800793f

Reference yield:

6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal (1033614-68-4) + methanesulfonyl chloride (124-63-0) → 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal (1033614-72-0)

Guidance literature:

With pyridine; In dichloromethane; at 0 ℃; for 16h; Inert atmosphere;

DOI:10.1021/ol800793f

upstream raw materials:

3-deoxy-3-(N-nosylamino)-D-gulal

C₂₀H₂₂N₂O₉S₂

Downstream raw materials:

6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

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