6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

Base Information

Chemical Name:6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal
CAS No.:1033614-72-0
Molecular Formula:C₃₂H₃₄N₄O₁₅S₃
Molecular Weight:810.838
Hs Code.:

Synonyms:6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

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Chemical Property of 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

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Technology Process of 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

There total 1 articles about 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1033614-68-4
6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal

: 124-63-0
methanesulfonyl chloride

: 1033614-72-0
6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 16h; Inert atmosphere;
DOI:10.1021/ol800793f

Reference yield: 73.0%

: 1033614-72-0
6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

: 67-63-0,8013-70-5
isopropyl alcohol

: 1033614-84-4
isopropyl 6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4'-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-2,3,4-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2-enopyranoside

Guidance literature:: With potassium carbonate; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol800793f

Reference yield:

: 1033614-66-2
3-deoxy-3-(N-nosylamino)-D-gulal

: 1033614-72-0
6-O-[6'-O-(benzyl)-2',3',4'-trideoxy-4-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-4-O-mesyl-3-deoxy-3-(N-nosylamino)-D-gulal

: 1033614-74-2
6-O-[6'-O-[6''-O-(benzyl)-2'',3'',4''-trideoxy-4''-(N-nosylamino)-α-D-erythro-hex-2''-enopyranosyl]-2',3',4'-trideoxy-4'-(N-nosylamino)-α-D-erythro-hex-2'-enopyranosyl]-3-deoxy-3-(N-nosylamino)-D-gulal

Guidance literature:: With potassium carbonate; In acetonitrile; at 20 ℃; for 24h; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol800793f