1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole

Base Information

Chemical Name:1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole
CAS No.:74644-93-2
Molecular Formula:C₂₅H₂₀N₂O₃
Molecular Weight:396.445
Hs Code.:

1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenz<c,d>indole

Synonyms:1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole

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Chemical Property of 1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole

Chemical Property:

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Technology Process of 1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole

There total 4 articles about 1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74606-98-7
2-benzoylamino-3-(1-benzoyl-2,3-dihydro-indol-3-yl)-propionic acid

: 74644-93-2
1-benzoyl-4-benzamido-5-oxo-1,2,2a,3,4,5-hexahydrobenzindole

Guidance literature:: With aluminium trichloride; acetic anhydride; Multistep reaction; 1.) 100 deg C, 15 min, 2.) ClCH₂-ClCH₂, reflux, 30 min;
DOI:10.1021/ja00536a067

Reference yield:

: 74606-98-7,88636-10-6,88636-11-7,88668-83-1,88668-84-2
(S)-2-Benzoylamino-3-(1-benzoyl-2,3-dihydro-1H-indol-3-yl)-propionic acid

: 74606-97-6,74644-93-2,88668-85-3
N-((S)-1-Benzoyl-5-oxo-1,2,2a,3,4,5-hexahydro-benzo[cd]indol-4-yl)-benzamide

Guidance literature:: With aluminium trichloride; acetic anhydride; Multistep reaction; 1.) 100 deg C, 15 min, 2.) ClCH₂-ClCH₂, reflux, 30 min;
DOI:10.1021/ja00536a067

Reference yield:

: 98-88-4
benzoyl chloride

: 74606-97-6,74644-93-2,88668-85-3
N-((S)-1-Benzoyl-5-oxo-1,2,2a,3,4,5-hexahydro-benzo[cd]indol-4-yl)-benzamide

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) Ac₂O, 2.) AlCl₃ / 1.) 100 deg C, 15 min, 2.) ClCH₂-ClCH₂, reflux, 30 min

With aluminium trichloride; acetic anhydride;
DOI:10.1021/ja00536a067