(E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

Base Information

Chemical Name:(E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine
CAS No.:1206713-19-0
Molecular Formula:C₁₈H₁₈BrN₃O₃S
Molecular Weight:436.329
Hs Code.:

Synonyms:(E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

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Technology Process of (E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

There total 5 articles about (E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 82657-76-9
1-(bromomethyl)-3-(methylsulfonyl)benzene

: 1173713-08-0
(E/Z)-N'-(4-bromo-2-cyano-5-hydroxyphenyl)-N,N-dimethylformimidamide

: 1206713-19-0
(E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

Guidance literature:: With potassium carbonate; In acetone; for 3h; Reflux;

Reference yield:

: 1173713-06-8
(E/Z)-N'-(4-bromo-2-cyano-5-methoxyphenyl)-N,N-dimethylformimidamide

: 1206713-19-0
(E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

Guidance literature:: Multi-step reaction with 2 steps

1: boron tribromide / dichloromethane / 20 h / 20 °C

2: potassium carbonate / acetone / 3 h / Reflux

With boron tribromide; potassium carbonate; In dichloromethane; acetone;

Reference yield:

: 10355-06-3
methyl 3-methylphenyl sulfone

: 1206713-19-0
(E/Z)-N'-[2-cyano-5-(3-methanesulphonylbenzyloxy)-4-bromophenyl]-N,N-dimethylformamidine

Guidance literature:: Multi-step reaction with 2 steps

1: 2,2'-azobis(isobutyronitrile); N-Bromosuccinimide / tetrachloromethane / 5 h / 25 °C / Reflux

2: potassium carbonate / acetone / 3 h / Reflux

With N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); potassium carbonate; In tetrachloromethane; acetone;