(2-Phenoxyethyl)triphenylphosphonium bromide

Base Information

Chemical Name:(2-Phenoxyethyl)triphenylphosphonium bromide
CAS No.:22409-83-2
Molecular Formula:C26H24 O P . Br
Molecular Weight:463.354
Hs Code.:2931900090
European Community (EC) Number:244-963-7
NSC Number:84063
DSSTox Substance ID:DTXSID00945063
Mol file:22409-83-2.mol

Synonyms:22409-83-2;(2-Phenoxyethyl)triphenylphosphonium bromide;(2-phenoxyethyl)(triphenyl)phosphonium bromide;2-phenoxyethyl(triphenyl)phosphanium;bromide;EINECS 244-963-7;NSC 84063;NSC84063;C26H24OP.Br;SCHEMBL4827493;C26-H24-O-P.Br;DTXSID00945063;QFIVZQJPMLZRIS-UHFFFAOYSA-M;NSC-84063;AKOS024318987;AB86699;(2-Phenoxyethyl)triphenylphosphoniumbromide;beta-phenoxyethyltriphenyl phosphonium-bromide;CS-0336352;FT-0638225;(2-Phenoxyethyl)(triphenyl)phosphanium bromide;C78067;(2-PHENOXYETHYL)(TRIPHENYL)PHOSPHONIUMBROMIDE

Suppliers and Price of (2-Phenoxyethyl)triphenylphosphonium bromide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
(2-PHENOXYETHYL)TRIPHENYLPHOSPHONIUM BROMIDE 95.00%
1G
$ 157.50

AHH
(2-Phenoxyethyl)(triphenyl)phosphoniumbromide 98%
5g
$ 678.00

Acrotein
(2-Phenoxyethyl)(triphenyl)phosphoniumbromide 97%
25g
$ 660.00

ACHEMBLOCK
(2-Phenoxyethyl)(triphenyl)phosphoniumbromide 95%
25G
$ 810.00

ACHEMBLOCK
(2-Phenoxyethyl)(triphenyl)phosphoniumbromide 95%
1G
$ 85.00

Total 11 raw suppliers

Chemical Property of (2-Phenoxyethyl)triphenylphosphonium bromide

Chemical Property:

Melting Point:103 °C
Boiling Point:°Cat760mmHg
Flash Point:°C
PSA：22.82000
Density:g/cm³
LogP:2.06350
Storage Temp.:Refrigerator
Solubility.:DMSO; Methanol
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:7
Exact Mass:462.07481
Heavy Atom Count:29
Complexity:380

Purity/Quality:

99% ^*data from raw suppliers

(2-PHENOXYETHYL)TRIPHENYLPHOSPHONIUM BROMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)OCC[P+](C2=CC=CC=C2)(C3=CC=CC=C3)C4=CC=CC=C4.[Br-]
Uses Triphenyl(2-phenoxyethyl)phosphonium Bromide is a useful reactant in organic synthesis.

Technology Process of (2-Phenoxyethyl)triphenylphosphonium bromide

There total 2 articles about (2-Phenoxyethyl)triphenylphosphonium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 589-10-6
phenoxyethyl bromide

: 108-95-2,27073-41-2
phenol

: 22409-83-2
(2-phenoxyethyl)triphenylphosphonium bromide

: [2-(Pyrrolidin-1-yl)ethyl]triphenylphosphonium bromide

Guidance literature:: With triphenylphosphine;

Reference yield:

: 589-10-6
phenoxyethyl bromide

: 603-35-0
triphenylphosphine

: 22409-83-2
(2-phenoxyethyl)triphenylphosphonium bromide

Guidance literature:: DOI:10.1039/j29700000671

Reference yield:

: 22409-83-2
(2-phenoxyethyl)triphenylphosphonium bromide

: 791-28-6
Triphenylphosphine oxide

Guidance literature:: Multi-step reaction with 4 steps

1: 76.9 percent / methanol / 72 h / 20 °C

2: 54 percent / aq. NaOH / benzene / 72 h / 20 °C

3: 72 percent / NH₂OH*HCl; Et₃N / CHCl₃ / 13 h / Heating

4: NaOMe / methanol / 1 h / 60 °C

With sodium hydroxide; hydroxylamine hydrochloride; sodium methylate; triethylamine; In methanol; chloroform; benzene;
DOI:10.1023/A:1021372009930