Technology Process of 1,3,4-tris(4-methoxyphenyl)-1H-pyrrole
There total 4 articles about 1,3,4-tris(4-methoxyphenyl)-1H-pyrrole which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium phosphate; copper(l) iodide; ethylenediamine;
In
toluene;
for 18h;
Schlenk technique;
Inert atmosphere;
Sealed tube;
Heating;
DOI:10.3184/174751917X15105690662863
- Guidance literature:
-
4-Methoxyphenylacetaldehyde; 4-methoxy-aniline;
In
tetrahydrofuran;
at 20 ℃;
for 0.5h;
Inert atmosphere;
With
silver(I) acetate; sodium acetate;
In
tetrahydrofuran;
at 60 ℃;
for 8h;
Inert atmosphere;
DOI:10.1021/ol1027877
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 24 h / 10 °C
2: chloroform-d1
With
sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water;
In
tetrahydrofuran; chloroform-d1; tert-butyl alcohol;
1: Lindgren oxidation;
DOI:10.1021/ol1027877
