1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

Base Information

Chemical Name:1,3,4-tris(4-methoxyphenyl)-1H-pyrrole
CAS No.:1261079-21-3
Molecular Formula:C₂₅H₂₃NO₃
Molecular Weight:385.463
Hs Code.:

Synonyms:1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

Suppliers and Price of 1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

There total 4 articles about 1,3,4-tris(4-methoxyphenyl)-1H-pyrrole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 2048-10-4
3,4-bis (4-methoxyphenyl)-1H-pyrrole

: 696-62-8
para-iodoanisole

: 1261079-21-3
1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

Guidance literature:: With potassium phosphate; copper(l) iodide; ethylenediamine; In toluene; for 18h; Schlenk technique; Inert atmosphere; Sealed tube; Heating;
DOI:10.3184/174751917X15105690662863

Reference yield: 77.0%

: 5703-26-4
4-Methoxyphenylacetaldehyde

: 104-94-9
4-methoxy-aniline

: 1261079-21-3
1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

Guidance literature:: 4-Methoxyphenylacetaldehyde; 4-methoxy-aniline; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

With silver(I) acetate; sodium acetate; In tetrahydrofuran; at 60 ℃; for 8h; Inert atmosphere;
DOI:10.1021/ol1027877

Reference yield:

: 1261079-22-4
1,3,4-tris(4-methoxyphenyl)-1H-pyrrole-2-carbaldehyde

: 1261079-21-3
1,3,4-tris(4-methoxyphenyl)-1H-pyrrole

Guidance literature:: Multi-step reaction with 2 steps

1: sodium dihydrogenphosphate; sodium chlorite; 2-methyl-but-2-ene; water / tetrahydrofuran; tert-butyl alcohol / 24 h / 10 °C

2: chloroform-d1

With sodium chlorite; sodium dihydrogenphosphate; 2-methyl-but-2-ene; water; In tetrahydrofuran; chloroform-d1; tert-butyl alcohol; 1: Lindgren oxidation;
DOI:10.1021/ol1027877