(4-n-Butylphenyl)diazo phenyl sulfide

Base Information

• Chemical Name: (4-n-Butylphenyl)diazo phenyl sulfide
• CAS No.: 134705-05-8
• Molecular Formula: C₁₆H₁₈N₂S
• Molecular Weight: 270.398
• Mol file: 134705-05-8.mol

Synonyms:(4-n-Butylphenyl)diazo phenyl sulfide

Chemical Property of (4-n-Butylphenyl)diazo phenyl sulfide

Chemical Property:

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Technology Process of (4-n-Butylphenyl)diazo phenyl sulfide

There total 1 articles about (4-n-Butylphenyl)diazo phenyl sulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-Butylaniline (104-13-2) + thiophenol (108-98-5) → (4-n-Butylphenyl)diazo phenyl sulfide (134705-05-8)

Guidance literature:

With hydrogenchloride; sodium nitrite; Yield given. Multistep reaction; 2) 2 deg C;

DOI:10.1021/jo00016a040

Reference yield: 54.0%

(4-n-Butylphenyl)diazo phenyl sulfide (134705-05-8) → 1-butylbenzene (104-51-8) + 4-(n-butyl)fluorobenzene (20651-65-4) + 1-Butyl-3-phenylsulfanyl-benzene + diphenyldisulfane (882-33-7)

Guidance literature:

With pyridine hydrogenfluoride; silver nitrate; In toluene; at 90 ℃; for 0.5h; Further byproducts given;

DOI:10.1021/jo00016a040

Reference yield: 54.0%

(4-n-Butylphenyl)diazo phenyl sulfide (134705-05-8) → 1-butylbenzene (104-51-8) + 3-Butyl-2-nitro-phenol + 1-Butyl-3-phenylsulfanyl-benzene + diphenyldisulfane (882-33-7)

Guidance literature:

With pyridine hydrogenfluoride; silver nitrate; In toluene; at 90 ℃; for 0.5h; Further byproducts given;

DOI:10.1021/jo00016a040

upstream raw materials:

4-Butylaniline

thiophenol

Downstream raw materials:

1-butylbenzene

4-(n-butyl)fluorobenzene

diphenyldisulfane