(1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene

Base Information

• Chemical Name: (1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene
• CAS No.: 169123-87-9
• Molecular Formula: C₁₈H₃₀OSi₂
• Molecular Weight: 318.607

Synonyms:(1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene

Chemical Property of (1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene

Chemical Property:

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Technology Process of (1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene

There total 1 articles about (1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

tert-butyldimethylsilyl chloride (18162-48-6) + {2-[2-(trimethylsilyl)ethynyl]phenyl}methanol (229027-92-3) → (1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene (169123-87-9)

Guidance literature:

With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 5h;

DOI:10.1021/jo901045g

Reference yield: 90.0%

(1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene (169123-87-9) → 1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-ethynylbenzene (173074-01-6)

Guidance literature:

With methanol; sodium sulfide; at 0 - 20 ℃; for 0.166667h; chemoselective reaction;

DOI:10.1016/j.tetlet.2015.04.104

Reference yield:

(1-(tert-butyldimethylsilanyloxy)methyl)-2-trimethylsilanylethynylbenzene (169123-87-9) → (2-{2-Methyl-2-phenylamino-1-[1-trimethylsilanyl-meth-(E)-ylidene]-propyl}-phenyl)-methanol

Guidance literature:

With methanol; tetrabutyl ammonium fluoride; Multistep reaction; 1.) 60 deg C;

DOI:10.1016/0040-4039(95)00741-T

upstream raw materials:

tert-butyldimethylsilyl chloride

{2-[2-(trimethylsilyl)ethynyl]phenyl}methanol

Downstream raw materials:

1-<<(tert-butyldimethylsilyl)oxy>methyl>-2-ethynylbenzene

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