3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane

Base Information

• Chemical Name: 3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane
• CAS No.: 1421834-78-7
• Molecular Formula: C₁₈H₃₃NO₂Si
• Molecular Weight: 323.551
• Mol file: 1421834-78-7.mol

Synonyms:3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane

Chemical Property of 3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane

There total 2 articles about 3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

3-(m-N,N-dimethylaminophenyloxy)propyl-trimethoxy silane (1421834-77-6) + 1-propylmagnesium chloride (2234-82-4) → 3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane (1421834-78-7)

Guidance literature:

In tetrahydrofuran; at 60 ℃; for 4h; Inert atmosphere;

Reference yield:

N,N-dimethyl-3-allyl-aniline (52276-05-8) → 3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane (1421834-78-7)

Guidance literature:

Multi-step reaction with 2 steps

1: bis(η2:η2-1,3-divinyltetramethyl)platinum(0) / tetrahydrofuran; toluene / 3 h / Inert atmosphere; Reflux

2: tetrahydrofuran / 4 h / 60 °C / Inert atmosphere

With bis(η2:η2-1,3-divinyltetramethyl)platinum(0); In tetrahydrofuran; toluene;

Reference yield: 19.0%

3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylmethoxy silane (1421834-78-7) + dihydroxy silicon(IV) phthalocyanine (19333-15-4) → {bis-[3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylsilyloxyl]}silicon(IV) phthalocyanine (1421834-79-8)

Guidance literature:

With 2-Ethylpyridine; for 4h; Reflux;

upstream raw materials:

3-(m-N,N-dimethylaminophenyloxy)propyl-trimethoxy silane

1-propylmagnesium chloride

N,N-dimethyl-3-allyl-aniline

Downstream raw materials:

{bis-[3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylsilyloxyl]}silicon(IV) phthalocyanine

{bis-[3-(m-N,N-dimethylaminophenyloxy)propyl-dipropylsilyloxy]}silicon(IV) phthalocyanine