Technology Process of C18H29NO2Si
There total 6 articles about C18H29NO2Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium iodide;
In
N,N-dimethyl-formamide;
at 0 - 20 ℃;
enantioselective reaction;
Inert atmosphere;
DOI:10.1055/s-0031-1290804
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / 0 °C
2: 1,3-bis-(diphenylphosphino)propane; cesium fluoride; palladium dichloride / water; benzene / 13 h / 20 - 65 °C / Inert atmosphere
3: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 2587.76 Torr
4: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C
5: sodium iodide / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; 1,3-bis-(diphenylphosphino)propane; hydrogen; triethylamine; cesium fluoride; trifluoroacetic acid; sodium iodide; palladium dichloride;
In
methanol; dichloromethane; water; N,N-dimethyl-formamide; benzene;
2: Suzuki-Miyaura coupling;
DOI:10.1055/s-0031-1290804
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 2587.76 Torr
2: trifluoroacetic acid / dichloromethane / 0.5 h / 0 °C
3: sodium iodide / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere
With
palladium 10% on activated carbon; hydrogen; trifluoroacetic acid; sodium iodide;
In
methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1055/s-0031-1290804
