6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

Base Information

Chemical Name:6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone
CAS No.:1225021-05-5
Molecular Formula:C₂₄H₁₇NO₅
Molecular Weight:399.403
Hs Code.:

Synonyms:6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

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Chemical Property of 6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

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Technology Process of 6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

There total 9 articles about 6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: cis-N-(4-hydroxyphenyl)-7-methoxyl-3-(4-methoxyphenyl)-1-oxo-1,2,3,4-tetrahydroisoquinoline-4-carboxylic acid

: 1225021-05-5
6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

Guidance literature:: cis-N-(4-hydroxyphenyl)-7-methoxyl-3-(4-methoxyphenyl)-1-oxo-1,2,3,4-tetrahydroisoquinoline-4-carboxylic acid; With thionyl chloride; In toluene; for 1.5h; Reflux;

With aluminum (III) chloride; In nitrobenzene; at 100 ℃; for 0.5h;

Reference yield:

: 123-30-8
4-amino-phenol

: 1225021-05-5
6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 4 h / Reflux

2.1: aluminum potassium sulfate dodecahydrate / acetonitrile / 12 h / 20 °C

3.1: thionyl chloride / toluene / 1.5 h / Reflux

3.2: 0.5 h / 100 °C

With thionyl chloride; aluminum potassium sulfate dodecahydrate; In ethanol; toluene; acetonitrile;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1225021-05-5
6-(4-hydroxyphenyl)-3,9-dimethoxy-5H-indeno[1,2-c] isoquinoline-5,11(6H)-diketone

Guidance literature:: Multi-step reaction with 3 steps

1.1: ethanol / 4 h / Reflux

2.1: aluminum potassium sulfate dodecahydrate / acetonitrile / 12 h / 20 °C

3.1: thionyl chloride / toluene / 1.5 h / Reflux

3.2: 0.5 h / 100 °C

With thionyl chloride; aluminum potassium sulfate dodecahydrate; In ethanol; toluene; acetonitrile;