1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane

Base Information

Chemical Name:1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane
CAS No.:77502-33-1
Molecular Formula:C28H20F6N4O2
Molecular Weight:558.4744
Hs Code.:
DSSTox Substance ID:DTXSID60998696

Synonyms:1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane;Benzamide, N,N'-(1,2-di-4-pyridinyl-1,2-ethanediyl)bis(4-(trifluoromethyl)-;N,N'-(1,2-Di-4-pyridinyl-1,2-ethanediyl)bis(4-(trifluoromethyl)benzamide);77502-33-1;DTXSID60998696;C28H20F6N4O2;C28-H20-F6-N4-O2;LS-26782;N,N'-[1,2-Di(pyridin-4-yl)ethane-1,2-diyl]bis[4-(trifluoromethyl)benzamide]

Suppliers and Price of 1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane

Chemical Property:

Boiling Point:726°Cat760mmHg
Flash Point:392.9°C
Density:1.37g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:10
Rotatable Bond Count:7
Exact Mass:558.14904487
Heavy Atom Count:40
Complexity:758

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C(=O)NC(C2=CC=NC=C2)C(C3=CC=NC=C3)NC(=O)C4=CC=C(C=C4)C(F)(F)F)C(F)(F)F

Technology Process of 1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane

There total 5 articles about 1,2-Bis(4-(trifluoromethyl)benzamido)-1,2-di-4-pyridylethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 77502-49-9
N-(1-Oxy-pyridin-4-ylmethyl)-4-trifluoromethyl-benzamide

: 56913-70-3
N-pyridin-4-ylmethyl-4-trifluoromethyl-benzamide

: 77502-33-1
C₂₈H₂₀F₆N₄O₂

Guidance literature:: With acetic anhydride; at 70 ℃; for 3h;
DOI:10.1002/jhet.5570200658

Reference yield: 38.0%

: 77502-49-9
N-(1-Oxy-pyridin-4-ylmethyl)-4-trifluoromethyl-benzamide

: 77502-33-1
C₂₈H₂₀F₆N₄O₂

Guidance literature:: In acetic anhydride; at 140 ℃; for 1.5h;
DOI:10.1002/jhet.5570180707

Reference yield:

: 3731-53-1
4-(aminomethyl)pyridine

: 77502-33-1
C₂₈H₂₀F₆N₄O₂

Guidance literature:: Multi-step reaction with 3 steps

1: dicyclohexylcarbodiimide / acetonitrile / 24 h / Ambient temperature

2: 80 percent / hydrogen peroxide (40 percent) / acetic acid / 80 °C

3: 38 percent / acetic anhydride / 1.5 h / 140 °C

With dihydrogen peroxide; dicyclohexyl-carbodiimide; In acetic anhydride; acetic acid; acetonitrile;
DOI:10.1002/jhet.5570180707