2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Base Information

Chemical Name:2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone
CAS No.:1257338-38-7
Molecular Formula:C₄₃H₃₉IN₂O₄
Molecular Weight:774.698
Hs Code.:

Synonyms:2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

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Chemical Property of 2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

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Technology Process of 2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

There total 2 articles about 2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 130296-37-6
N-(1-hexylheptyl)-perylene-3,4,9,10-tetracarboxylic-3,4-carboximide-9,10-anhydride

: 540-37-4
p-aminoiodobenzene

: 1257338-38-7
2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:: With 1H-imidazole; zinc diacetate; at 140 ℃; for 3h;
DOI:10.1021/ja101544x

Reference yield: 35.0%

: 22513-16-2
1-hexylheptylamine

: 128-69-8
perylene-3,4,9,10-tetracarboxylic acid 3,4:9,10-dianhydride

: 540-37-4
p-aminoiodobenzene

: 1257338-38-7
2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:: With 1H-imidazole; at 130 ℃; for 2h; Inert atmosphere;
DOI:10.1021/jo500945k

Reference yield: 95.0%

: 1257338-38-7
2-(1-hexylheptyl)-9-(4-iodophenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

: 1066-54-2
trimethylsilylacetylene

: 1257338-42-3
2-(1-hexylheptyl)-9-(4-trimethylsilanylethynylphenyl)anthra[2,1,9-def;6,5,10-d'e'f']diisoquinoline-1,3,8,10-tetraone

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; triphenylphosphine; In tetrahydrofuran; for 16h; Inert atmosphere;
DOI:10.1021/ja101544x