di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]

Base Information

Chemical Name:di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]
CAS No.:85478-07-5
Molecular Formula:C₄₂H₃₈O₄P₂Pd₂
Molecular Weight:881.549
Hs Code.:

Synonyms:di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]

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Chemical Property of di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]

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Technology Process of di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]

There total 1 articles about di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 19.0%

: 3375-31-3
palladium diacetate

: 7650-91-1
benzyldiphenylphosphane

: 85478-07-5
di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]

Guidance literature:: In methanol; methanol soln. of Pd(OAc)2 and PBzPh2 (contg. BzPh2P=O) refluxed for 3 h; evapd., chromd. (SiO2, CH2Cl2/Et2O), evapd., recrystd. from CH2Cl2 and hexane;
DOI:10.1016/S0020-1693(00)83572-0

Reference yield: 86.0%

: 85478-07-5
di-μ-acetato-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]

: di-μ-chloro-bis[(2-(diphenylphosphinomethyl)phenyl-C1,P)palladium(II)]-acetone (2/1)

Guidance literature:: With acetone; lithium chloride; In water; acetone; mixt. of educt and LiCl in acetone/H2O stirred for 1 d at room temp.; ppt. collected, washed with methanol/water; elem. anal.;
DOI:10.1016/S0020-1693(00)83572-0