N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide

Base Information

• Chemical Name: N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide
• CAS No.: 186753-11-7
• Molecular Formula: C₁₅H₁₈I₃N₃O₇
• Molecular Weight: 733.037

Synonyms:N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide

Chemical Property of N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide

Chemical Property:

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Technology Process of N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide

There total 1 articles about N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.5%

formic acid (64-18-6) + 5-amino-N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (76801-93-9) → N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide (186753-11-7)

Guidance literature:

With acetic anhydride; at 2.5 - 20 ℃; Inert atmosphere;

Reference yield: 48.0%

N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide (186753-11-7) + 5--N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide (171897-76-0) → 5-(3-(N-(3,5-bis(2,3-dihydroxypropylcarbamoyl)-2,4,6-triiodophenyl)formamido)-2-hydroxypropylamino)-N1,N3-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Guidance literature:

With potassium hydroxide; In methanol; water; at 20 ℃; pH=11.3-11.5;

Reference yield: 43.0%

N,N'-bis(2,3-dihydroxypropyl)-5-formylamino-2,4,6-triiodoisophthalamide (186753-11-7) + 1,2:3,4-Diepoxybutane (564-00-1,1464-53-5,30031-64-2,30419-67-1,34897-03-5,298-18-0) → 5,5'-(2,3-dihydroxybutane-1,4-diyl)bis(formylazanediyl)bis(N1,N3-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide)

Guidance literature:

With boric acid; potassium hydroxide; In methanol; water; pH=12.6-13;

upstream raw materials:

formic acid

5-amino-N,N'-bis(2,3-dihydroxypropyl)-2,4,6-triiodoisophthalamide

Downstream raw materials:

C₃₁H₃₆I₆N₆O₁₄

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