C₂₈H₂₃ClF₆N₂O₃S

Base Information

Chemical Name:C₂₈H₂₃ClF₆N₂O₃S
CAS No.:1415576-14-5
Molecular Formula:C₂₈H₂₃ClF₆N₂O₃S
Molecular Weight:617.012
Hs Code.:

C<sub>28</sub>H<sub>23</sub>ClF<sub>6</sub>N<sub>2</sub>O<sub>3</sub>S

Synonyms:C₂₈H₂₃ClF₆N₂O₃S

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₈H₂₃ClF₆N₂O₃S

Chemical Property:

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Technology Process of C₂₈H₂₃ClF₆N₂O₃S

There total 9 articles about C₂₈H₂₃ClF₆N₂O₃S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1415578-03-8
C₂₂H₂₂F₃NO₃S

: 69045-84-7
2,3-dichloro-5-trifluoromethylpyridine

: 1415576-14-5
C₂₈H₂₃ClF₆N₂O₃S

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 70 ℃; for 2h;

Reference yield:

: 76041-72-0
2-mercapto-5-trifluoromethylpyridine

: 1415576-14-5
C₂₈H₂₃ClF₆N₂O₃S

Guidance literature:: Multi-step reaction with 7 steps

1.1: triethylamine / tetrahydrofuran / 1.5 h / 0 °C / Cooling with ice

2.1: chloroform / 8 h / 0 °C

3.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

3.2: 0.5 h / Reflux

4.1: water; sodium carbonate / 5 h / Reflux

5.1: dmap / chloroform; toluene / 1 h / 75 °C / Inert atmosphere

6.1: acetic acid; hydrogen bromide / 0.5 h / 100 °C

7.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 70 °C

With dmap; water; hydrogen bromide; sodium methylate; sodium carbonate; caesium carbonate; acetic acid; triethylamine; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide; toluene; 2.1: |Wittig Olefination;

Reference yield:

: 114449-80-8
C₉H₈F₃NOS

: 1415576-14-5
C₂₈H₂₃ClF₆N₂O₃S

Guidance literature:: Multi-step reaction with 6 steps

1.1: chloroform / 8 h / 0 °C

2.1: sodium methylate / tetrahydrofuran; methanol / 0.25 h / Reflux

2.2: 0.5 h / Reflux

3.1: water; sodium carbonate / 5 h / Reflux

4.1: dmap / chloroform; toluene / 1 h / 75 °C / Inert atmosphere

5.1: acetic acid; hydrogen bromide / 0.5 h / 100 °C

6.1: caesium carbonate / N,N-dimethyl-formamide / 2 h / 70 °C

With dmap; water; hydrogen bromide; sodium methylate; sodium carbonate; caesium carbonate; acetic acid; In tetrahydrofuran; methanol; chloroform; N,N-dimethyl-formamide; toluene; 1.1: |Wittig Olefination;