1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

Base Information

Chemical Name:1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane
CAS No.:781626-13-9
Molecular Formula:C₂₃H₃₀O₄Si
Molecular Weight:398.574
Hs Code.:

Synonyms:1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

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Chemical Property of 1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

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Technology Process of 1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

There total 4 articles about 1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 781626-12-8
1-methoxy-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

: 1-(4-methoxyphenyl)vinyllithium

: 781626-13-9
1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

Guidance literature:: 1-(4-methoxyphenyl)vinyllithium; In hexane; at 20 ℃; for 0.166667h;

1-methoxy-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane; In hexane; at 20 - 30 ℃; for 16.5h;

With silica gel (32-63 μm, ICN 02826); In hexane; for 0.0333333h;

Reference yield: 47.0%

: 781626-12-8
1-methoxy-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

: 100-06-1
1-(4-methoxyphenyl)ethanone

: 781626-13-9
1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

Guidance literature:: 1-(4-methoxyphenyl)ethanone; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 2,4,6-triisopropylbenzenesulfonylhydrazone; In hexane; at -78 - 20 ℃;

1-methoxy-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane; In hexane; at 20 ℃; for 16h;
DOI:10.1016/j.bmcl.2005.12.062

Reference yield:

: 2406-34-0
1,1-dichloro-1-silacyclohexane

: 781626-13-9
1-[1-(4-methoxyphenyl)vinyl]-1-(2,4,6-trimethoxyphenyl)-1-silacyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; 1,2-bis(dimethylamino)ethane / hexane / 72 h / 20 °C

1.2: hexane / 6 h / 20 °C

1.3: 66 percent / hexane / 16 h / 20 °C

2.1: n-butyllithium; 2,4,6-triisopropylbenzenesulfonylhydrazone; 1,2-bis(dimethylamino)ethane / hexane / -78 - 20 °C

2.2: 47 percent / hexane / 16 h / 20 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; 2,4,6-triisopropylbenzenesulfonylhydrazone; In hexane;
DOI:10.1016/j.bmcl.2005.12.062