diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate

Base Information

Chemical Name:diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate
CAS No.:1242450-42-5
Molecular Formula:C₃₆H₃₉N₈O₆PSi
Molecular Weight:738.815
Hs Code.:

Synonyms:diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate

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Technology Process of diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate

There total 1 articles about diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1242450-41-4
N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

: 22400-41-5
diphenyl [(triphenylphosphoranylidene)methyl]phosphonate

: 1242450-42-5
diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate

Guidance literature:: In dimethyl sulfoxide; at 20 ℃; for 10h;
DOI:10.5012/bkcs.2010.31.6.1643

Reference yield: 96.0%

: 1242450-42-5
diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate

: 1242450-44-7
diphenyl (E)-2-((2R,3S,4R,5R)-5-(6-amino-9H-purin-9-yl)-4-azido-3-hydroxy-tetrahydrofuran-2-yl)vinylphosphonate

Guidance literature:: diphenyl (E)-2-((2R,3S,4R,5R)-4-azido-5-(6-benzamido-9H-purin-9-yl)-3-(tert-butyldime-thylsilyloxy)-tetrahydrofuran-2-yl)vinylphosphonate; With hydrogenchloride; water; In ethanol; at 60 ℃; for 11h;

With sodium hydrogencarbonate; In ethanol; water; Cooling;
DOI:10.5012/bkcs.2010.31.6.1643