N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

Base Information

Chemical Name:N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide
CAS No.:1242450-41-4
Molecular Formula:C₂₃H₃₀N₈O₄Si
Molecular Weight:510.628
Hs Code.:

Synonyms:N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

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Technology Process of N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

There total 2 articles about N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 1242450-40-3
N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5-((tert-butyldimethyl silyloxy)methyl)-tetrahydrofuran-2-yl)-9H-purin-6-yl)-N-benzoylbenzamide

: 1242450-41-4
N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

Guidance literature:: With water; trifluoroacetic acid; at 0 ℃; for 3h;
DOI:10.5012/bkcs.2010.31.6.1643

Reference yield: 86.0%

: 1245200-31-0
6-N-benzoyl-2′-azido-3′,5′-bis-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 1242450-41-4
N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

Guidance literature:: With trifluoroacetic acid; In tetrahydrofuran; water; at 0 ℃; for 18h;
DOI:10.1002/anie.201001473

Reference yield:

: 1242450-41-4
N-(9-((2R,3R,4S,5R)-3-azido-4-(tert-butyldimethylsilyloxy)-5(hydroxymethyl) tetrahydro-furan-2-yl)-9H-purin-6-yl)benzamide

: C₂₃H₂₈N₈O₄Si

Guidance literature:: With pyridinium trifluroacetate; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dimethyl sulfoxide; at 20 ℃; for 24h;
DOI:10.5012/bkcs.2010.31.6.1643