4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Base Information

Chemical Name:4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside
CAS No.:1021496-49-0
Molecular Formula:C₆₃H₇₀Cl₃NO₁₅
Molecular Weight:1187.61
Hs Code.:

4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Synonyms:4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

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Chemical Property of 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

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Technology Process of 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

There total 1 articles about 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1021496-21-8
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-3-O-allyl-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

: 1021496-49-0
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

Guidance literature:: palladium dichloride; In methanol; dichloromethane; at 20 ℃;
DOI:10.1016/j.tet.2008.01.093

Reference yield: 55.0%

: 64-18-6
formic acid

: 1021496-49-0
4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside

: 1021496-20-7
4-methoxyphenyl 3-acetamido-3-deoxy-α-D-fucopyranosyl-(1->2)-β-D-rhamnopyranosyl-(1->3)-α-D-rhamnopyranoside

Guidance literature:: 4-methoxyphenyl 2,4-di-O-benzyl-3-deoxy-3-(2,2,2-trichloroethoxycarbonylamino)-α-D-fucopyranosyl-(1->2)-4-O-benzyl-β-D-rhamnopyranosyl-(1->3)-2,4-di-O-benzyl-α-D-rhamnopyranoside; With acetic anhydride; copper; acetic acid; zinc; at 20 ℃; for 72h;

formic acid; palladium on activated charcoal; In methanol; for 2h; Further stages.;
DOI:10.1016/j.tet.2008.01.093